Published October 8, 2024
| Version v1
Dataset
Open
Oxyresveratrol datasets
Creators
Description
Continuous Rotation (Anhydrate_Oxyresveratrol) | |
Project | NanED (www.naned.eu) |
Instrumental | |
Instrument | Zeiss Libra 120 |
Radiation source | LaB6 |
Accelerating voltage | 120 kV |
Wavelength | 0.0335 Å |
Probe Type | Nanodiffraction |
Beam Diameter | 600 nm |
Beam Convergence | Parallel beam |
Detector | Timepix Single Electron Detector |
Number of pixels in the image | 512 x 512 |
Physical pixel size | 55 µm * 55 µm |
Effective camera length | 180 mm |
Calibration constant | 0.006027 Å-1/pixel |
Sample description | |
Name | Anhydrate Oxyresveratrol |
Chemical composition | C14H12O4 |
Sample source | Sigma |
Sample preparation | Crushed between two glass slides before deposition on a Cu grid. |
Experimental | |
Data type | 3D Electron Diffraction (3D ED) |
Data collection method | Continuous Rotation Electron Diffraction (CRED) |
Rotation Speed | 1.12º/s |
Temperature | 293 K |
Number of crystals contributing to the dataset | 1 |
Number of experimental frames | 199 |
Tilt range, tilt step | -54.85º to +60.49º |
Exposure time per frame | 500ms |
Software | |
Software used for data collection | WinTEM (Zeiss), LibraEDT |
Software used for processing | Pets2 |
Software used for solution | Shelxt |
Software used for refinement | Jana2020 |
Precession: | |
Instrumental | |
Instrument | Zeiss Libra 120 |
Radiation source | LaB6 |
Accelerating voltage | 120 kV |
Wavelength | 0.0335 Å |
Probe Type | Nanodiffraction |
Beam Diameter | 150 nm |
Beam Convergence | Parallel beam |
Detector | Timepix Single Electron Detector |
Number of pixels in the image | 512 x 512 |
Physical pixel size | 55 µm * 55 µm |
Effective camera length | 144 mm |
Calibration constant | 0.006027 Å-1/pixel |
Sample description | |
Name | Hydrate Oxyresveratrol |
Chemical composition | C14H12O4.2H2O |
Sample source | Sigma |
Sample preparation | Cryoplunge freezing |
Experimental | |
Data type | 3D Electron Diffraction (3D-ED) |
Data collection method | Precession |
Precession Semiangle | 1º |
Temperature | 93 K |
Number of crystals contributing to the dataset | 1 |
Number of experimental frames | 91 |
Tilt range, tilt step | -30º to +60, 1º |
Exposure time per frame | 1s |
Software | |
Software used for data collection | WinTEM (Zeiss), Digistar (NanoMEGAS) and Sophy (Software for Physics) |
Software used for processing | PETS2 |
Software used for solution | SIR2019 |
Software used for refinement | Jana2020 |
Files
Oxyresveratrol_dataset.zip
Files
(42.8 MB)
Name | Size | Download all |
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md5:e63e24f27c1ce22e3581c161df26ac90
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