Barriers to Resolution in 1H NMR of Rotating Solids

The NMR raw data is in both jcamp and topspin format. The data folders are separated according to the samples.

For the 2MeIm (2-methylimidazole) spectra:

- dilution and deuteration tests with 1D, CP, HETCOR and DQ/SQ

For the HMB (hexamethylbenzene) spectra:

- dilution tests with 1D, CP, HETCOR and DQ/SQ

- variable MAS dataset for 1D, T2' and DQ/SQ

For the ZIF-8 (zeolitic imidazolate framework) spectra:

- dilution tests with 1D, CP, HETCOR and DQ/SQ

- variable MAS dataset for T2'  (the  variable 1D spectra correspond to the first increment of the T2' experiment) and DQ/SQ

For the L-Tyrosine.HCl spectra:

- variable MAS dataset for 1D, T2' and DQ/SQ

For the PS (polystyrene) spectra:

- variable MAS dataset for 1D, T2' and DQ/SQ

Matlab scripts:

- rmseval_conv_1pe (peak fitting script to a voigt function type)

- rmseval_gls_1pe (peak fitting script to a GLS function type)

- conv_2d_simu_clean_2023 (simulation of 2D peaks with Gaussian, Tilted Gaussian and Lorentzian shapes)

- fitting_hmb_antidiag_scaled_2023 (example with HMB data to extract the antidiagonal from a DQ/SQ spectrum and fit to GLS or Voigt)