A Rapid Method of Analysis of Halo-Nitrosyl Complexes of Rhenium

Inorganic Chemistry Laboratory, University College of Science, Calcutta-9

Received 20 April, 1972

The hydrogen combustion technique of Ter Meulen has been effectively modified and extended to the analysis of nitric oxide-halogen complexes of rheniurn. The analysis of a variety of compounds show that simultaneous determination of rheniurn, alkali :metals, nitric oxide along with several organic amines and halogens is possible in a single determination.