Reproducibility and Scalability of Magnetic Nanoheater Synthesis - Supplementary Information

The following are available online at https://www.mdpi.com/article/10.3390/nano11082059/s1: Experimental procedures for the characterization of MNP’s and comparison among the scaled and the standard experiment. Figure S1. Temperature profiles for the scaled-up experiments; Figure S2. Measurements of the successive AMF heating and cooling cycles for selected samples, showing the effects of the progressive destabilization of the colloids; Figure S3. XRD diffraction patterns of all samples; Figure S4. Hysteresis cycles at room temperature of all the samples as measured and corrected for the content of organic matter measured by TG-ATD; Figure S5. Particle size distributions of all the samples and solvodynamic size distributions of their dispersions in toluene determined by PCS in number and in volume; Figure S6. Results of the magnetothermal experiments at 286 kHz 18 kA/m and 92 kHz 50 kA/m for all the samples. Table S1. Average parameters of the temperature profiles for each boiling time, averages of all the experiments, and their repeatability; Table S2. Experimental data of scaled-up samples. Reproducibility r = (1 − σ/x¯) · 100. Error of the average: 1.96 · σ/√N (95% confidence). N = 6.