Published February 26, 2024
| Version v1
Dataset
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Epidote - Sample 1 NanED Round Robin, Data: ESR11
Description
Epidote
The following submission contains the data collection of datasets for the sample epidote under the NanED round-robin project. 5 single crystals were identified, and the continuous rotation data acquisition technique was used to collect datasets. All the datasets were processed with REDp, XDS and shelx software. The table below summarizes the data collection parameters for the datasets.
Continuous Rotation:
General information | |
Project | NanED (www.naned.eu) |
ESR Project | ESR11 - Round Robin |
Project Label | RR-1 |
Sample Label | RR-1_SU |
Dataset Label | RR-1_SU_11-1 to 5 |
Instrumental | |
Instrument | Transmission electron microscope JEOL 2100 LaB6 |
Radiation source | LaB6 |
Accelerating voltage | 200 kV |
Wavelength | 0.0251 Å |
Probe type | Parallel beam |
Beam diameter | 6 μm |
Beam convergence | Parallel beam, convergence <0.1 mrad |
Detector | Hybrid pixel detector ASI Timepix (bottom mounted) |
Number of pixels in the image | 512 x 512 |
Pixel size | 55 µm x 55 µm |
Effective camera length | See cRED_log.txt in each dataset |
Calibration constant | 0.004990 Å-1/pixel |
Sample description | |
Name | Epidote |
Chemical composition |
Ca2FexAl3-xSi3O13H |
Sample source | Natural source from Val d'Ossola, Italy |
Sample preparation | Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film |
Experimental | |
Data Type | Electron diffraction data - 3D ED |
Data collection method | Continuous Rotation |
Temperature (K) used during data collection | 293 K |
Number of crystals contributing to the data set | 5 |
Number of experimental frames | See cRED_log.txt in each dataset |
Tilt range, tilt step, tilt per frame | See cRED_log.txt in each dataset |
Exposure time per frame | See cRED_log.txt in each dataset |
Software | |
Software used for the data collection | Instamatic |
Software used for processing | XDS |
Authorship and bibliography | |
Author(s) of the data | Angelina Vypritskaia (ESR 11) |
Related data | |
Publication(s) | |
Files and data formats | |
Images folder |
RED: Folder containing images of the diffraction pattern from each frame (mrc) SMV/data: Folder containing images of the diffraction pattern from each frame (img) |
Image format | mrc and img |
Additional folders/files | tiff image: image of the crystal |
cRED_log: log file of data collection | |
1.ed3d: input file for REDp | |
XDS.INP: input file for the program XDS |
Notes
Files
RR-1_SU_11.zip
Files
(1.7 GB)
Name | Size | Download all |
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md5:8c4c3c72bcc06db1a0435a1420d7aee5
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1.7 GB | Preview Download |
Additional details
Funding
- NanED – Electron Nanocrystallography 956099
- European Commission