Published February 26, 2024 | Version v1
Dataset Open

Epidote - Sample 1 NanED Round Robin, Data: ESR11

  • 1. ROR icon Stockholm University

Description

Epidote

The following submission contains the data collection of datasets for the sample epidote under the NanED round-robin project. 5 single crystals were identified, and the continuous rotation data acquisition technique was used to collect datasets. All the datasets were processed with REDp, XDS and shelx software. The table below summarizes the data collection parameters for the datasets. 

 

Continuous Rotation:

General information  
Project NanED (www.naned.eu)
ESR Project ESR11 - Round Robin
Project Label RR-1
Sample Label RR-1_SU
Dataset Label RR-1_SU_11-1 to 5
   
Instrumental  
Instrument Transmission electron microscope JEOL 2100 LaB6
Radiation source LaB6
Accelerating voltage 200 kV
Wavelength 0.0251 Å
Probe type Parallel beam
Beam diameter 6 μm
Beam convergence Parallel beam, convergence <0.1 mrad
Detector Hybrid pixel detector ASI Timepix (bottom mounted)
Number of pixels in the image 512 x 512
Pixel size 55 µm x 55 µm
Effective camera length See cRED_log.txt in each dataset
Calibration constant 0.004990 Å-1/pixel
   
Sample description  
Name Epidote
Chemical composition

Ca2FexAl3-xSi3O13H

Sample source Natural source from Val d'Ossola, Italy
Sample preparation Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film
   
Experimental  
Data Type Electron diffraction data - 3D ED
Data collection method Continuous Rotation
Temperature (K) used during data collection 293 K
Number of crystals contributing to the data set 5
Number of experimental frames See cRED_log.txt in each dataset
Tilt range, tilt step, tilt per frame See cRED_log.txt in each dataset
Exposure time per frame See cRED_log.txt in each dataset
   
Software  
Software used for the data collection Instamatic
Software used for processing XDS
   
Authorship and bibliography  
Author(s) of the data Angelina Vypritskaia (ESR 11) 
Related data  
Publication(s)  
   
Files and data formats  
Images folder

RED: Folder containing images of the diffraction pattern from each frame (mrc)

SMV/data: Folder containing images of the diffraction pattern from each frame (img)

Image format mrc and img
Additional folders/files tiff image: image of the crystal
  cRED_log: log file of data collection
  1.ed3d: input file for REDp
  XDS.INP: input file for the program XDS

Notes

*Project Label "RR1" stands for Round Robin 1

Files

RR-1_SU_11.zip

Files (1.7 GB)

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md5:8c4c3c72bcc06db1a0435a1420d7aee5
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Additional details

Funding

NanED – Electron Nanocrystallography 956099
European Commission