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Published September 30, 2022 | Version v1
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Bioactive prenylated phenolic compounds from the aerial parts of Glycyrrhiza uralensis

Creators

  • 1. ** & * & State Key Laboratory of Natural and Biomimetic Drugs, School of Pharmaceutical Sciences, Peking University, 38 Xueyuan Road, Beijing, 100191, China

Description

Hasan, Aobulikasimu, Zhang, Meng, Shang, Zhan-Peng, Yi, Yang, Kuang, Yi, Yu, Rong, Fan, Jing-Jing, Huang, Yu-Xi, Nijat, Dilaram, Qiao, Xue, Ye, Min (2022): Bioactive prenylated phenolic compounds from the aerial parts of Glycyrrhiza uralensis. Phytochemistry (113284) 201: 1-9, DOI: 10.1016/j.phytochem.2022.113284, URL: http://dx.doi.org/10.1016/j.phytochem.2022.113284

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LSID
urn:lsid:plazi.org:pub:4550FFD0FF83FFBE064EFF90EE5CFFEC

Related works

Has part
Figure: 10.5281/zenodo.8236857 (DOI)
Figure: 10.5281/zenodo.8236859 (DOI)
Figure: 10.5281/zenodo.8236861 (DOI)
Figure: 10.5281/zenodo.8236863 (DOI)
Figure: 10.5281/zenodo.8236865 (DOI)

References

  • Glycyuralin Q (1). Yellow crystals; mp 175-177 °C; [α]D 25 0 (c 0.06, MeOH); UV (MeOH) λ max (log ε) 282 (2.18), 314 (2.22) nm; IR (KBr) ν max 3376, 2922, 2854, 1608, 1475, 1360, 1286, 1268, 1159, 1067, 1001 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 1; ( )-HRESIMS m/ z 393.1706 [M-H]- (calcd for C24H25O5, 393.1697).
  • Glycyuralin R (2). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 258 (1.53), 354 (1.30) nm; IR (KBr) ν max 3329, 2949, 2837, 1647, 1449, 1408, 1113, 1014, 518 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 1; ( )-HRESIMS m/z 401.1232 [M-H]- (calcd for C21H21O8, 401.1231).
  • Glycyuralin S (3). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 258 (2.00), 355 (1.91) nm; IR (KBr) ν max 3270, 1647, 1470, 1356, 1296, 1216, 1015, 418 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 1; ( )-HRESIMS m/z 415.1395 [M-H]- (calcd for C22H23O8, 415.1387).
  • Glycyuralin T (4). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 257 (3.43), 376 (3.44) nm; IR (KBr) ν max 3373, 2771, 1679, 1650, 1481, 1368, 1319, 1284, 1202, 1024, 999, 824 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 1; ( )-HRESIMS m/z 387.1083 [M-H]- (calcd for C20H19O8, 387.1078).
  • Glycyuralin U (5). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 269 (2.29) nm; IR (KBr) ν max 3373, 2926, 1590, 1459, 1377, 1278, 1207, 1141, 982, 727 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 2; ( )-HRESIMS m/z 379.1911 [M-H]- (calcd for C24H27O4, 379.1904).
  • Glycyuralin V (6). White, amorphous powder; [α]D 25 +13 (c 0.05, MeOH); UV (MeOH) λ max (log ε) 280 (2.36) nm; IR (KBr) ν max 3352, 2924, 1678, 1593, 1497, 1431, 1369, 1284, 1203, 1139, 1047, 1022, 992, 827 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 2; ( )-HRESIMS m/z 397.2015 [M-H]- (calcd for C24H29O5, 397.2014).
  • Glycyuralin W (7). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 257 (2.12) nm, 376 (2.13) nm; IR (KBr) ν max 3390, 2913, 1650, 1593, 1484, 1446, 1371, 1276, 1200, 1157, 1118, 802 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 2; ( )-HRESIMS m/z 369.0974 [M-H]- (calcd for C20H17O7, 369.0969).
  • Glycyuralin X (8). Yellow, amorphous powder; UV (MeOH) λ max (log ε) 281 (2.12) nm; IR (KBr) ν max 394, 2926, 1673, 1593, 1491, 1436, 1375, 1335, 1288, 1200, 1143, 997, 840 cm 1; 1H and 13C NMR (DMSO- d6) data, Table 2; ( )-HRESIMS m/z 327.1599 [M-H]- (calcd for C20H23O4, 327.1596).