SYNTHESIS AND INVESTIGATING OF THE NOVEL OF ES-PANI@PDNPSNANOCOMPOSITE
- 1. Departement of Chemistry, Faculty of Mathematics and Natural Sciences Jember University, Jl. Kalimantan 37, Jember 681752.
- 2. Departement of Chemistry, Faculty of Mathematics and Natural Sciences Gadjah Mada University, Jl. Sekip Utara, Yogyakarta 55281.
Description
The aim of this research is the synthesize materials Novel of ES-PANI@PdNPs nanocomposites obtained chemically. The synthesis of ES-PANI@PdNPs nanocomposite was prepared by the chemical method using FeCl3 as a redox initiator (insitu) and refluxed for 48 hours at 500C, then dried at 500C for 24 hours, obtained a brown-black solid and no water-soluble.The nanocomposite is characterized by UV-Vis and Fourier transform infrared (FTIR) spectroscopy, the composite shows absorption of Pd(0) nanoparticles along with ES-PANI peaks at 312 nm. FTIR and UV-visible spectra show an interaction between Pd(0) and ES-PANI. This indicated that Pd(0) zero valence had been formed and that internal reduction processes had occurred by imines and amines toward Pd(II) ions.
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