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Published August 10, 2021 | Version v1
Journal article Open

Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry

  • 1. Department of Chemical Engineering and Chemistry, Eindhoven University of Technology
  • 2. van 't Hoff Institute for Molecular Sciences (HIMS), Universiteit van Amsterdam

Description

Photoinduced chemical transformations have received in recent years a tremendous amount of attention, providing a plethora of opportunities to synthetic organic chemists. However, performing a photochemical transformation can be quite a challenge because of various issues related to the delivery of photons. These challenges have barred the widespread adoption of photochemical steps in the chemical industry. However, in the past decade, several technological innovations have led to more reproducible, selective, and scalable photoinduced reactions. Herein, we provide a comprehensive overview of these exciting technological advances, including flow chemistry, high-throughput experimentation, reactor design and scale-up, and the combination of photo- and electro-chemistry.

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acs.chemrev.1c00332.pdf

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Additional details

Funding

FlowPhotoChem – Heterogenous Photo(electro)catalysis in Flow using Concentrated Light: modular integrated designs for the production of useful chemicals 862453
European Commission