Published September 25, 2020 | Version 1
Dataset Open

FIB-tomography data of porous Zr-oxide fabricated with varying sintering conditions

  • 1. ZHAW, Zurich University of Applied Sciences, Winterthur

Description

This dataset contains 3D data acquired with FIB-tomography from porous Zr-oxide. The pore structures of the ceramic materials were investigated in context with optimization of transport properties (aimed for low viscous flow/permeability and high electric conduction via liquid electrolyte in the pores), so that the Zr-oxide is suitable for application as liquid junction (diaphragm) in pH-sensors. Further details on the scientific background are given in Holzer et al., 2016, Materials & Design, 99, 314–327. (http://doi.org/10.1016/j.matdes.2016.03.034).

 

The tomographs represent 9 ceramic materials that were produced with different sintering temperatures (1250, 1300, 1325 and 1350°C) and different sintering times (1, 2 and 3 hours). The study includes quantitative descriptions of relevant microstructure characteristics (porosity, tortuosity, constrictivity, hydraulic radius) and corresponding effective transport prorperties (permeability, conductivity).

 

Each tomograph is presented as stack of 2D-tiff-images in two different versions: as gray-scale images (raw data) and as binarized images (segmented, with solid=black and pores=white). The voxel resolution is 10x10x10 nm for all 18 image stacks.

 

More details on the image data (e.g. voxel nr, image window size, data size) are given in the downloadable file '2_3D_Data_Info.xlsx'.

Notes

> Funding: Swiss Commission for Technology and Innovation (CTI), Project Nr. 16851.1 PFNM-NM > Project Database: https://www.zhaw.ch/no_cache/en/research/research-database/project-detailview/projektid/2106/ > Authors Personal Homepages: https://www.zhaw.ch/en/about-us/person/holz/ https://www.zhaw.ch/index.php?id=9118 https://www.researchgate.net/profile/Lorenz_Holzer https://scholar.google.com/citations?hl=de&user=9Wr7IccAAAAJ

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10_ZY3_00X_1325_3h_RawData.zip

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Additional details

Related works

Is documented by
Journal article: 10.1016/j.matdes.2016.03.034 (DOI)