Published November 14, 2022
| Version 1.0.0
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Synthesis of both Enantiomers of 3-Hydroxydodecanedioic Acid
Description
Experimental procedures for the preparation of
Diethyl decanedioate
Diethyl 3-oxododecanedioate
Diethyl rac-3-hydroxydodecanedioate
Diethyl (R)-3-hydroxydodecanedioate
Diethyl(S)-3-hydroxydodecanedioate
(R)-3-Hydroxydodecanedioic acid and (S)-3-hydroxydodecanedioic acid
are reported. Data such as 1H-NMR, 13C-NMR, Rf values, FT.IR, and HRMS data are reported. Copies of NMR spectra are provided. Mosher analyses of compounds are provided.
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SI_Synthesis_of_3_hydroxydodecandioic_acid.pdf
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Additional details
Related works
- Is described by
- Publication: 10.1016/j.celrep.2025.115357 (DOI)
- Is supplemented by
- Dataset: 10.5517/ccdc.csd.cc2g080s (DOI)