Published December 18, 2024 | Version v1
Dataset Open

Dataset for publication "(Bi)carbonate Precipitation and Gas Diffusion Electrode Stability Coexist during Pulsed Electrochemical CO2 Reduction"

  • 1. ROR icon Swiss Federal Laboratories for Materials Science and Technology
  • 2. ROR icon ETH Zurich
  • 3. ROR icon European Synchrotron Radiation Facility
  • 4. EDMO icon ETH Zürich

Description

Broad topic: continuous and pulsed electrochemical reduction of CO2 using Cu-based gas diffusion electrodes in neutral electrolyte, operando characterisation using synchrotron radiation (wide-angle X-ray scattering), (bi)carbonate precipitation.

Data is divided in subfolders named after the figure of the paper.

Raw data, processed data, and Origin/PowerPoint files are all contained in the subfolders.

Synchrotron raw data are linked to the experiment numbers MA5874 and INHC1776 at ESRF

A subfolder corresponding to a sample contains: data from a potentiostat, gas chromatograms, recording of flow, pressure and temperature, tables of calculated Faradaic efficiency (FE), png image of the FE vs t, zipped raw files, and integrated synchrotron data. 

.json file was created using a yadg scheme (https://dgbowl.github.io/yadg/master/index.html), and data was processed by a dgpost scheme (https://dgbowl.github.io/dgpost/master/index.html)

Synchrotron data are analysized using this python library https://github.com/EmpaEconversion/Twaxs

Files

Data_for_submission.zip

Files (2.8 GB)

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md5:ffec240e25ef68fec7be86b23a436e2d
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Additional details

Funding

Swiss National Science Foundation
Ambizione PZ00P2_215992
Swiss National Science Foundation
NCCR Catalysis 180544
Board of the Swiss Federal Institutes of Technology
Synthetic Fuels from Renewable Resources Joint Strategic Initiative
Board of the Swiss Federal Institutes of Technology
“PREMISE”: Open and Reproducible Materials Science Research Open Research Data Program