Natrolite - Sample 2 NanED Round Robin, Data: ESR10
Description
Natrolite
The following submission contains the data collection and processing of the dataset for the sample natrolite under the NanEd round-robin project. A single crystal was identified, and the rotation data acquisition technique was used to collect the dataset on the same crystal. The dataset was processed with XDS software. The table below summarizes the data collection parameters for the dataset. The following data is also in the data folder as a Word file.
Continuous Rotation:
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General information: |
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Project |
NanED (www.naned.eu) |
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ESR Project |
ESR10 - Round Robin |
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Project Label |
RR-2 |
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Sample Label |
RR-2_SU |
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Data set Label |
RR-2 |
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Instrumental: |
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Instrument |
Transmission electron microscope JEOL 2100 LaB6 |
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Radiation source |
LaB6 |
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Accelerating voltage |
200 kV |
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Wavelength |
0.0251 Å |
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Probe Type |
Parallel beam |
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Beam Diameter |
6 μm |
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Beam Convergence |
Parallel beam, convergence <0.1mrad |
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Detector |
Hybrid pixel detector ASI Timepix (bottom mounted) |
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Number of pixels in the image |
512 x 512 |
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Pixel size |
55 µm x 55 µm |
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Effective camera length |
250 mm |
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Calibration constant |
0.004990 Å-1/pixel |
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Sample description: |
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Name |
Natrolite |
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Chemical composition |
Na2Si3Al2O10.(H2O)2 |
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Sample source |
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Sample preparation |
Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film |
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Experimental: |
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Data Type |
Electron diffraction data - 3D ED |
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Data collection method |
Continuous Rotation |
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Temperature (K) used during data collection |
293 K |
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Number of crystals contributing to the data set |
1 |
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Number of experimental frames |
513 |
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tilt range, tilt step, tilt per frame |
-48.35°-70.58°, 0.453°/s, 0.2318°/frame |
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Exposure time per frame |
0.5 |
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Software: |
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Software used for the data collection |
Instamatic |
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Software used for processing |
XDS |
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Authorship and bibliography |
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Author(s) of the data |
Lei Wang (ESR 10) |
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Related data |
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Publication(s) |
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Files and data formats |
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Image folder |
REDp: Folder containing images of the diffraction pattern from each frame XDS: Folder containing images of the diffraction pattern from each frame |
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Image format |
mrc and img |
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Additional folders/files |
Crystal image : image of the crystal |
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cRED_log: log file of data collection |
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1.ed3d: input file for REDp |
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XDS.INP: input file for the program XDS |
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Notes: *Project Label "RR-2" stands for Round Robin 2 *RR-2 contains 1 dataset. |
Files
Natrolite_4_datasets.zip
Files
(876.6 MB)
| Name | Size | Download all |
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md5:57df518bbc01c16feab6017103475abb
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876.6 MB | Preview Download |