Published May 7, 2024
| Version v2
Dataset
Open
3D ED dataset of 1,3,5-triphenylbenzene
Authors/Creators
Description
Continuous rotation 3D ED data collection of 1,3,5-triphenylbenzene (TPB). See the following table for additional details.
| Project name | TPB_25032024 |
| Instrumental | |
| Instrument | ELDICO ED-1 electron diffractometer |
| Electron source |
LaB6 |
| Electron energy | 160 kV |
| Wavelength | 0.02851 Å |
| Beam mode | pseudo-parallell |
| Beam diameter | 750 nm |
| Detector | Dectris QUADRO |
| Detetor no. of pixels | 512 x 512 |
| Detetor pixel size | 75 µm |
| Data collection mode | continuous rotation |
| Measurement temperature | 298 K |
| Instrument control software | eldix, Version 4.3.1 |
| Sample | |
| Compound | 1,3,5-triphenylbenzene |
| Chemical formula |
C24H18 |
| Sample source | commercial, 99+% purity |
| Grid | amorphous carbon on copper |
| Sample preparation | grinding of the sample between microscope slides and dry preparation on the grid |
| Files and data formats | |
| Diffraction frame folders | 03, 06, 07, 08 |
| Diffraction frame format | .cbf |
| Additional files | subfolders with STEM images of the particles at different tilt angles |
| Comments | folder _full.zip contains the full measurement data, folder _recommended.zip already has frames removed which are affected by other crystals in the beam, shadowing by the grid bars, or beam damage |
Files
TPB_25032024_full.zip
Files
(235.1 MB)
| Name | Size | Download all |
|---|---|---|
|
md5:c8ccb5e1b2312d950b4a7331b71b1852
|
127.2 MB | Preview Download |
|
md5:f3493bb425a7e313b003176cd8b9a19d
|
107.9 MB | Preview Download |
Additional details
Dates
- Submitted
-
2024-05-06
- Collected
-
2024-03-25
- Updated
-
2024-05-07