Published April 7, 2023 | Version v2

Imaging the footprint of nanoscale electrochemical reactions for assessing synergistic hydrogen evolution

  • 1. Universite Paris Cite
  • 2. CNRS, Universite Paris Cite
  • 3. Universite Paris CIte

Description

Dataset complementary to supporting information, such as optical movies, COMSOL model, and Python codes to analyze the experimental and simulated data according to the manuscript submitted for publication.
The movies correspond to cyclic voltammetry operando monitoring by optical microscopy of the reduction of water + KCl in the presence of NiCl2 at an ITO electrode or NiCl2 or MgCl2 at ITO electrode coated with Pt nanoparticles.

The python function was used to extract the halo size around each nanoparticle from optical images, the python routines were used to postprocess the COMSOL simulation and evalaute the simulated halo size.

Files

86_r198nm.txt

Files (869.1 MB)

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Additional details

Related works

Is supplement to
Journal article: 10.1002/anie.202304950 (DOI)

Funding

Agence Nationale de la Recherche
SEAM - Science and Engineering for Advanced Materials and devices ANR-10-LABX-0096
European Commission
SENTINEL - Single-Entity NanoElectrochemistry 812398
Agence Nationale de la Recherche
PIRaNa - Quantitative imaging of hydroxyl radical production at nano-objects: an opto-electrochemical methodology. ANR-20-CE42-0001