Published July 31, 2020 | Version v1
Journal article Open

Engineering of silicone-based mixtures for the digital light processing of Åkermanite scaffolds

  • 1. Centre for Functional and Surface-Functionalized Glass, Alexander Dubček University of Trenčín, 911 50 Trenčín, Slovakia
  • 2. Ceramics Department, National Research Centre, Cairo, Egyp
  • 3. Joint Glass Centre of the IIC SAS, TnUAD, and FChFT STU, FunGlass, Alexander Dubček University of Trenčín, Trenčín, Slovakia
  • 4. Department of Industrial Engineering, Università degli Studi di Padova, Padova, Italy

Description

Siliconesmixedwithoxidefillersareinterestingprecursorsforseveralbioactiveglass-ceramics.Akeypointisrepresentedbythecouplingofsynthesisandshaping,sincehighlyporousbodies,informoffoamsorscaffolds,arefirstmanufacturedwithsiliconesinthepolymericstate,atlowtemperature,andlatersubjectedtoceramictransformation. After successful application of direct ink writing, the present study illustrates the tuning ofsilicone-based mixtures in order to form åkermanite (Ca2MgSi2O7) reticulated scaffolds by digital light pro-cessing.Thisimpliedtheselectionofcommercialsilicones,producingstableandhomogeneousblendswithaphotocurable resin and enabling the manufacturing of defect-free printed scaffolds, before and after firing,withoutfillers.Theblendswerefurtherrefinedwiththeintroductionoffillers,followedbyfiringat1100°C,inair.Optimizedsamples(fromH44resin)andreactivefillers(includingupto4.5wt.%boraxadditive),ledtocrack-freeandphase-purescaffoldswithmicroporousstruts.

Files

Engineering of silicone-based mixtures for the digital light processing of Åkermanite scaffolds.pdf

Additional details

Funding

European Commission
FunGlass - Centre for functional and surface-functionalized glasses 739566