Published December 21, 2021 | Version 1.0

XCT data of metallic feedstock powder with pore size analysis

  • 1. Bundesanstalt für Materialforschung und –prüfung (BAM)

Description

X-Ray computed tomography (XCT) scan of 11 individual metallic powder particles, made of (Mn,Fe)2(P,Si) alloy

The data set consists of 4 single XCT scans which have been stitched together [3] after reconstruction.
The powder material is an (Mn,Fe)2(P,Si) alloy with an average density of 6.4 g/cm³. The particle size range is about 100 - 150 µm with equivalent pore diameters up to 75 µm. The powder and the metallic alloy are described in detail in [1, 2].

Data acquisition

The data was acquired using a Zeiss Xradia 620 Versa X-ray microscope which provides the opportunity of optical magnification.

Tomographic imaging parameters
XCT system Zeiss Xradia 620 Versa
Voltage 80 kV
Power 10 W
Source filtering "LE2" (system specific) -
Source-object distance 10 mm
Object-detector distance 10 mm
Geom. magnification 2 -
Optical magnification 20 -
Native pixel size 13.5 µm
Binning 2x2 px
Voxel size 0.68 µm
No. of projections per scan 801 1
No. of scans 4 -
Exposure time per projection 5 s

 

Projection data (801 single TIFF-files each):

  • proj_00
  • proj_01
  • proj_02
  • proj_03

Reconstructed data:

  • raw-volume (MnFePSi-Powder_80kV_10W_LE2_20x_5s_801_0p68_BHC=2_Stitch_U16_966x1020x2916.raw + header.txt)
  • analyzed data as Volume Graphics Studio MAX 3.4.5 project

Stitched 2D data (images stitched with ImageJ-Plugin described in [3]:

  • Stitched_0deg_Projections.tif
  • Pores+Particles_Analysis.tif

 

[1] G.-R. Jaenisch, U. Ewert, A. Waske, and A. Funk, “Radiographic Visibility Limit of Pores in Metal Powder for Additive Manufacturing,” Metals, vol. 10, no. 12, p. 1634, Dec. 2020. https://doi.org/10.3390/met10121634

[2] X. Miao et al., “Printing (Mn,Fe)2(P,Si) magnetocaloric alloys for magnetic refrigeration applications,” J. Mater. Sci., vol. 55, no. 15, pp. 6660–6668, May 2020. https://doi.org/10.1007/s10853-020-04488-8

[3] S. Preibisch, S. Saalfeld, and P. Tomancak, “Globally optimal stitching of tiled 3D microscopic image acquisitions,” Bioinformatics, vol. 25, no. 11, pp. 1463–1465, Jun. 2009.

Files

Analyzed_Data_VG.zip

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Additional details

Related works

Cites
Journal article: 10.3390/met10121634 (DOI)
Journal article: 10.1007/s10853-020-04488-8 (DOI)
Journal article: 10.1093/bioinformatics/btp184 (DOI)

References

  • G.-R. Jaenisch, U. Ewert, A. Waske, and A. Funk, "Radiographic Visibility Limit of Pores in Metal Powder for Additive Manufacturing," Metals (Basel)., vol. 10, no. 12, p. 1634, Dec. 2020.
  • X. Miao et al., "Printing (Mn,Fe)2(P,Si) magnetocaloric alloys for magnetic refrigeration applications," J. Mater. Sci., vol. 55, no. 15, pp. 6660–6668, May 2020
  • Stephan Preibisch, Stephan Saalfeld, Pavel Tomancak, Globally optimal stitching of tiled 3D microscopic image acquisitions, Bioinformatics, Volume 25, Issue 11, 1 June 2009, Pages 1463–1465, https://doi.org/10.1093/bioinformatics/btp184