XCT data of metallic feedstock powder with pore size analysis
Authors/Creators
- 1. Bundesanstalt für Materialforschung und –prüfung (BAM)
Description
X-Ray computed tomography (XCT) scan of 11 individual metallic powder particles, made of (Mn,Fe)2(P,Si) alloy
The data set consists of 4 single XCT scans which have been stitched together [3] after reconstruction.
The powder material is an (Mn,Fe)2(P,Si) alloy with an average density of 6.4 g/cm³. The particle size range is about 100 - 150 µm with equivalent pore diameters up to 75 µm. The powder and the metallic alloy are described in detail in [1, 2].
Data acquisition
The data was acquired using a Zeiss Xradia 620 Versa X-ray microscope which provides the opportunity of optical magnification.
| XCT system | Zeiss Xradia 620 Versa | |
| Voltage | 80 | kV |
| Power | 10 | W |
| Source filtering | "LE2" (system specific) | - |
| Source-object distance | 10 | mm |
| Object-detector distance | 10 | mm |
| Geom. magnification | 2 | - |
| Optical magnification | 20 | - |
| Native pixel size | 13.5 | µm |
| Binning | 2x2 | px |
| Voxel size | 0.68 | µm |
| No. of projections per scan | 801 | 1 |
| No. of scans | 4 | - |
| Exposure time per projection | 5 | s |
Projection data (801 single TIFF-files each):
- proj_00
- proj_01
- proj_02
- proj_03
Reconstructed data:
- raw-volume (MnFePSi-Powder_80kV_10W_LE2_20x_5s_801_0p68_BHC=2_Stitch_U16_966x1020x2916.raw + header.txt)
- analyzed data as Volume Graphics Studio MAX 3.4.5 project
Stitched 2D data (images stitched with ImageJ-Plugin described in [3]:
- Stitched_0deg_Projections.tif
- Pores+Particles_Analysis.tif
[1] G.-R. Jaenisch, U. Ewert, A. Waske, and A. Funk, “Radiographic Visibility Limit of Pores in Metal Powder for Additive Manufacturing,” Metals, vol. 10, no. 12, p. 1634, Dec. 2020. https://doi.org/10.3390/met10121634
[2] X. Miao et al., “Printing (Mn,Fe)2(P,Si) magnetocaloric alloys for magnetic refrigeration applications,” J. Mater. Sci., vol. 55, no. 15, pp. 6660–6668, May 2020. https://doi.org/10.1007/s10853-020-04488-8
[3] S. Preibisch, S. Saalfeld, and P. Tomancak, “Globally optimal stitching of tiled 3D microscopic image acquisitions,” Bioinformatics, vol. 25, no. 11, pp. 1463–1465, Jun. 2009.
Files
Analyzed_Data_VG.zip
Files
(12.2 GB)
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Additional details
Related works
- Cites
- Journal article: 10.3390/met10121634 (DOI)
- Journal article: 10.1007/s10853-020-04488-8 (DOI)
- Journal article: 10.1093/bioinformatics/btp184 (DOI)
References
- G.-R. Jaenisch, U. Ewert, A. Waske, and A. Funk, "Radiographic Visibility Limit of Pores in Metal Powder for Additive Manufacturing," Metals (Basel)., vol. 10, no. 12, p. 1634, Dec. 2020.
- X. Miao et al., "Printing (Mn,Fe)2(P,Si) magnetocaloric alloys for magnetic refrigeration applications," J. Mater. Sci., vol. 55, no. 15, pp. 6660–6668, May 2020
- Stephan Preibisch, Stephan Saalfeld, Pavel Tomancak, Globally optimal stitching of tiled 3D microscopic image acquisitions, Bioinformatics, Volume 25, Issue 11, 1 June 2009, Pages 1463–1465, https://doi.org/10.1093/bioinformatics/btp184