Published November 6, 2020 | Version v1

Structure Determination of Boron-Based Oxidative Dehydrogenation Heterogeneous Catalysts With Ultrahigh Field 35.2 T 11B Solid-State NMR Spectroscopy

  • 1. Department of Chemistry, Iowa State University, Ames, Iowa 50011, United States; Ames Laboratory, US Department of Energy, Ames, Iowa 50011, United States
  • 2. Department of Chemistry, University of Wisconsin - Madison, Madison, Wisconsin 53706, United States
  • 3. National High Magnetic Field Laboratory (NHMFL), Tallahassee, Florida 32310, United States
  • 4. Department of Chemical and Biological Engineering, University of Wisconsin - Madison, Madison, Wisconsin 53706, United States
  • 5. Department of Chemistry and Department of Chemical and Biological Engineering, University of Wisconsin - Madison, Madison, Wisconsin 53706, United States

Description

Pulse sequences, raw 1D and 2D NMR data for main text figures.

Notes

Materials synthesis and solid-state NMR spectroscopy (R.W.D., M.C.C, N.R.A., W.P.M., I.H. and A.J.R.) was supported by the National Science Foundation under Grant No. CBET-1916809. This study made use of the National High Magnetic Field Laboratory to perform solid-state NMR experiments. The National High Magnetic Field Laboratory is supported by the National Science Foundation through NSF/DMR-1644779 and the State of Florida. Development of the SCH magnet and NMR instrumentation was supported by NSF (DMR-1039938 and DMR-0603042) and NIH P41 GM122698.

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