Published December 15, 2023 | Version ver1.0

XPS spectra for Li intercalated few-layer MoS2 films

Authors/Creators

  • 1. CNR-IOM, Istituto Officina dei Materiali, Trieste, Italy

Contributors

Project member:

  • 1. CNR-IOM, Istituto Officina dei Materiali, TriesteCNR-IOM, Istituto Officina dei Materiali, Trieste, Italy
  • 2. Institute of Electrical Engineering, SAS, Bratislava, Slovakia

Description

Description

Dataset for synchrotron-based x-ray photoelectron (XPS) spectra of Li doped MoS2 nanofilms grown on c-plane sapphire substrate by two techniques: thermally assisted conversion (TAC) and pulsed laser deposition (PLD). Reference spectra for undoped MoS2 were measured on a commercial MoS2 powder sample.

 

Data formats

The XPS datasets are available in two formats.

  1. VAMAS (ASCII ISO 14976).
  2. Plain text column files: Double-column files (dat) and corresponding metadata files (txt).

Methods

Sample preparation

MoS2 nanofilms were synthesized using two techniques:

  1. Thermally assisted conversion (TAC) of 1-nm-thick Mo by one-zone sulfurization.
  2. Pulsed laser deposition (PLD).

Lithium was incorporated into the as-prepared MoS2 films by solid-state diffusion during the subsequent sulfurization process, where a part of sulfur powder was replaced by lithium sulfide (Li2S) as a source of Li.

Notes

Data were acquired at BACH beamline, Elettra synchrotron facility. Access was provided by IOM-CNR in Trieste (Italy) within the framework of the NFFA-Europe Pilot Transnational Access Activity, proposal ID101. 

Files

XPS-Li-MoS2-PLD-synthesis.zip

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Additional details

Related works

Is supplement to
Journal article: 10.1063/5.0191046 (DOI)
Journal article: https://zenodo.org/records/10813107 (Other)

Funding

European Commission
NEP - Nanoscience Foundries and Fine Analysis - Europe|PILOT 101007417