MoS2@C3F6 Raw data Fitting data 1T-MoS2 (d5) 1T-MoS2 (d3) 2H-MoS2 (d5) 2H-MoS2 (D3) MoO2 (d5) MoO2 (d3) MoO3 (d5) MoO3 (d3) S (2s) Binding Energy (eV) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) Intensity (a.u.) 240.18 -152.948 -20.162 -20.1789 -20.1789 -20.1789 -20.1789 -20.1789 -20.1789 -20.1789 -20.162 -20.1789 240.08 90.3092 -20.152 -20.1791 -20.1791 -20.1791 -20.1791 -20.1791 -20.1791 -20.1791 -20.152 -20.1791 239.98 2.10226 -20.136 -20.1792 -20.1792 -20.1792 -20.1792 -20.1792 -20.1792 -20.1792 -20.136 -20.1792 239.88 -127.258 -20.1111 -20.1794 -20.1794 -20.1794 -20.1794 -20.1794 -20.1794 -20.1794 -20.1111 -20.1794 239.78 81.7806 -20.0763 -20.1831 -20.1831 -20.1831 -20.1831 -20.1831 -20.1831 -20.1831 -20.0763 -20.1831 239.68 118 -20.0231 -20.1889 -20.1889 -20.1889 -20.1889 -20.1889 -20.1889 -20.1889 -20.0231 -20.1889 239.58 244.652 -19.939 -20.1939 -20.1939 -20.1939 -20.1939 -20.1939 -20.1939 -20.1939 -19.939 -20.1939 239.48 -57.3247 -19.8142 -20.2026 -20.2026 -20.2026 -20.2026 -20.2026 -20.2026 -20.2026 -19.8142 -20.2026 239.38 149.471 -19.6252 -20.2116 -20.2116 -20.2116 -20.2116 -20.2116 -20.2116 -20.2116 -19.6252 -20.2116 239.28 111.95 -19.3429 -20.2203 -20.2203 -20.2203 -20.2203 -20.2203 -20.2203 -20.2203 -19.3429 -20.2203 239.18 91.9944 -18.9258 -20.2269 -20.2269 -20.2269 -20.2269 -20.2269 -20.2269 -20.2269 -18.9258 -20.2269 239.08 79.8086 -18.3222 -20.2341 -20.2341 -20.2341 -20.2341 -20.2341 -20.2341 -20.2341 -18.3222 -20.2341 238.98 -3.23974 -17.4575 -20.2421 -20.2421 -20.2421 -20.2421 -20.2421 -20.2421 -20.2421 -17.4575 -20.2421 238.88 201.27 -16.2311 -20.2501 -20.2501 -20.2501 -20.2501 -20.2501 -20.2501 -20.2501 -16.2311 -20.2501 238.78 122.522 -14.509 -20.2581 -20.2581 -20.2581 -20.2581 -20.2581 -20.2581 -20.2581 -14.509 -20.2581 238.68 86.1867 -12.1166 -20.2668 -20.2668 -20.2668 -20.2668 -20.2668 -20.2668 -20.2668 -12.1166 -20.2668 238.58 132.088 -8.82506 -20.276 -20.276 -20.276 -20.276 -20.276 -20.276 -20.276 -8.82507 -20.276 238.48 31.6347 -4.33963 -20.2839 -20.2839 -20.2839 -20.2839 -20.2839 -20.2839 -20.2839 -4.33965 -20.2839 238.38 109.079 1.70917 -20.2927 -20.2927 -20.2927 -20.2927 -20.2927 -20.2927 -20.2927 1.70914 -20.2927 238.28 185.534 9.78649 -20.3017 -20.3017 -20.3017 -20.3017 -20.3017 -20.3017 -20.3016 9.78644 -20.3017 238.18 103.704 20.4607 -20.3153 -20.3153 -20.3153 -20.3153 -20.3153 -20.3153 -20.3152 20.4606 -20.3153 238.08 478.826 34.4268 -20.3338 -20.3338 -20.3338 -20.3338 -20.3338 -20.3338 -20.3337 34.4267 -20.3338 237.98 405.621 52.5202 -20.3537 -20.3537 -20.3537 -20.3537 -20.3537 -20.3537 -20.3534 52.5199 -20.3537 237.88 205.317 75.719 -20.3733 -20.3733 -20.3733 -20.3733 -20.3733 -20.3733 -20.3728 75.7185 -20.3733 237.78 174.966 105.148 -20.3944 -20.3944 -20.3944 -20.3944 -20.3944 -20.3944 -20.3935 105.147 -20.3944 237.68 205.733 142.08 -20.415 -20.415 -20.415 -20.415 -20.415 -20.415 -20.4136 142.078 -20.415 237.58 450.212 187.915 -20.4337 -20.4337 -20.4337 -20.4337 -20.4337 -20.4337 -20.4312 187.913 -20.4337 237.48 257.847 244.146 -20.4558 -20.4558 -20.4558 -20.4558 -20.4558 -20.4558 -20.4516 244.142 -20.4558 237.38 460.567 312.314 -20.4834 -20.4834 -20.4834 -20.4834 -20.4834 -20.4834 -20.4765 312.307 -20.4834 237.28 591.435 393.938 -20.5165 -20.5165 -20.5165 -20.5165 -20.5165 -20.5165 -20.5051 393.927 -20.5165 237.18 622.014 490.418 -20.5526 -20.5526 -20.5526 -20.5526 -20.5526 -20.5526 -20.5339 490.4 -20.5526 237.08 668.734 602.901 -20.5975 -20.5975 -20.5975 -20.5975 -20.5975 -20.5975 -20.5673 602.871 -20.5975 236.98 929.291 732.147 -20.6494 -20.6494 -20.6494 -20.6494 -20.6494 -20.6494 -20.601 732.099 -20.6494 236.88 989.448 878.354 -20.7093 -20.7093 -20.7093 -20.7093 -20.7093 -20.7093 -20.6325 878.277 -20.7093 236.78 1197.34 1040.98 -20.7777 -20.7777 -20.7777 -20.7777 -20.7777 -20.7777 -20.6569 1040.85 -20.7777 236.68 1261.08 1218.55 -20.8574 -20.8574 -20.8574 -20.8573 -20.8574 -20.8573 -20.669 1218.36 -20.8574 236.58 1518.79 1408.54 -20.9489 -20.9489 -20.9489 -20.9487 -20.9489 -20.9485 -20.6578 1408.25 -20.9489 236.48 1824.73 1607.25 -21.0567 -21.0567 -21.0567 -21.0561 -21.0567 -21.0552 -20.6108 1606.8 -21.0567 236.38 2211.2 1809.78 -21.1776 -21.1776 -21.1776 -21.1764 -21.1776 -21.1736 -20.5011 1809.1 -21.1776 236.28 2194.29 2010.13 -21.3154 -21.3154 -21.3154 -21.3129 -21.3154 -21.3044 -20.2981 2009.1 -21.3154 236.18 2537.29 2201.42 -21.4668 -21.4668 -21.4668 -21.4615 -21.4668 -21.4378 -19.9506 2199.87 -21.4668 236.08 2536.17 2376.24 -21.629 -21.629 -21.629 -21.6183 -21.629 -21.5558 -19.3896 2373.92 -21.6289 235.98 2644.67 2527.2 -21.8003 -21.8003 -21.8003 -21.7791 -21.8003 -21.6228 -18.5225 2523.72 -21.8003 235.88 2899.88 2647.45 -21.9798 -21.9798 -21.9798 -21.9384 -21.9798 -21.5658 -17.2251 2642.24 -21.9798 235.78 2815.71 2731.42 -22.1634 -22.1634 -22.1634 -22.084 -22.1634 -21.2346 -15.3279 2723.58 -22.1634 235.68 2839.85 2775.4 -22.3507 -22.3507 -22.3507 -22.2011 -22.3507 -20.3471 -12.6116 2763.51 -22.3506 235.58 2811.87 2778.08 -22.5387 -22.5387 -22.5387 -22.2622 -22.5387 -18.3828 -8.78679 2759.89 -22.5386 235.48 2702.97 2740.96 -22.7239 -22.7239 -22.7239 -22.2221 -22.7239 -14.4348 -3.47953 2712.93 -22.7239 235.38 2689.5 2668.56 -22.9064 -22.9064 -22.9064 -22.0116 -22.9064 -7.01073 3.78307 2625.08 -22.9063 235.28 2601.1 2568.44 -23.0846 -23.0846 -23.0846 -21.5183 -23.0846 6.21539 13.598 2500.9 -23.0845 235.18 2526.73 2451.03 -23.2584 -23.2584 -23.2584 -20.5656 -23.2584 28.6331 26.706 2346.48 -23.2582 235.08 2466.98 2329.21 -23.4293 -23.4293 -23.4293 -18.8832 -23.4293 64.8112 44.0119 2168.98 -23.4291 234.98 2493.14 2217.64 -23.5942 -23.5942 -23.5942 -16.0569 -23.5942 120.332 66.6126 1975.97 -23.5939 234.88 2231.61 2131.56 -23.7534 -23.7532 -23.7534 -11.4811 -23.7534 201.088 95.8054 1774.88 -23.753 234.78 2169.83 2084.89 -23.9077 -23.9071 -23.9077 -4.28487 -23.9077 311.826 133.102 1572.53 -23.9071 234.68 2154.33 2087.77 -24.0584 -24.0567 -24.0584 6.75279 -24.0584 453.832 180.227 1374.78 -24.0575 234.58 2193.65 2143.46 -24.2053 -24.2008 -24.2053 23.2998 -24.2053 622.054 239.112 1186.37 -24.204 234.48 2203.59 2245.95 -24.3522 -24.3408 -24.3522 47.5622 -24.3522 802.634 311.849 1010.83 -24.3505 234.38 2241.33 2379.68 -24.4994 -24.4708 -24.4994 82.3762 -24.4994 972.593 400.652 850.532 -24.4969 234.28 2178.59 2523.24 -24.6491 -24.58 -24.6491 131.251 -24.6491 1103.43 507.753 706.779 -24.6457 234.18 2354.39 2657.22 -24.8037 -24.6411 -24.8037 198.352 -24.8037 1169 635.294 579.993 -24.7991 234.08 2558.38 2773.54 -24.9648 -24.594 -24.9648 288.381 -24.9648 1154.85 785.164 469.878 -24.9584 233.98 2691.34 2881.05 -25.136 -24.3152 -25.136 406.293 -25.136 1064.12 958.804 375.603 -25.1272 233.88 3005.35 3003.73 -25.3213 -23.5583 -25.3213 556.827 -25.3213 916.226 1156.98 295.964 -25.3093 233.78 3239.09 3172.32 -25.5203 -21.8453 -25.5203 743.801 -25.5203 739.207 1379.52 229.54 -25.504 233.68 3392.81 3414.07 -25.7364 -18.3011 -25.7363 969.177 -25.7364 560.351 1625.08 174.799 -25.7143 233.58 3842.68 3745.22 -25.9745 -11.373 -25.9744 1231.94 -25.9745 399.673 1890.85 130.195 -25.9447 233.48 4358.58 4168.01 -26.2377 1.59566 -26.2374 1526.97 -26.2377 267.812 2172.4 94.2416 -26.1976 233.38 4898.16 4671.65 -26.5304 24.969 -26.5298 1844.08 -26.5303 167.309 2463.55 65.5532 -26.4767 233.28 5461.59 5235.46 -26.8563 65.6315 -26.855 2167.64 -26.8562 95.3742 2756.44 42.8771 -26.7847 233.18 5902.26 5833.47 -27.2176 133.982 -27.2148 2477.11 -27.2172 46.645 3041.66 25.1085 -27.1223 233.08 6510.63 6439.6 -27.6118 245.009 -27.6059 2748.76 -27.6106 15.2176 3308.74 11.2959 -27.4855 232.98 6845.14 7033.29 -28.0408 419.187 -28.0288 2958.63 -28.0372 -4.18919 3546.7 0.62824 -27.874 232.88 7522.93 7604.85 -28.504 682.829 -28.4799 3086.26 -28.4938 -15.7394 3744.81 -7.56937 -28.2844 232.78 8035.23 8159.18 -29.0029 1067.23 -28.9557 3118.36 -28.9757 -22.436 3893.5 -13.8534 -28.715 232.68 8604.06 8716.25 -29.5428 1605.85 -29.4516 3051.47 -29.4728 -26.2944 3985.19 -18.6779 -29.1666 232.58 9597.76 9306.68 -30.1302 2328.7 -29.9573 2892.6 -29.9574 -28.5851 4015.02 -22.4079 -29.6404 232.48 10437 9961.76 -30.7619 3253.47 -30.4402 2657.88 -30.3514 -30.0552 3981.36 -25.3224 -30.1266 232.38 10861.8 10698.6 -31.4425 4373.82 -30.8545 2369.41 -30.505 -31.1317 3885.99 -27.6451 -30.6211 232.28 11718.3 11503.4 -32.1743 5646.84 -31.1193 2051.45 -30.1159 -32.0429 3733.87 -29.5471 -31.1164 232.18 12477 12319.1 -32.9532 6984.17 -31.0941 1726.92 -28.6071 -32.8998 3532.67 -31.1518 -31.5954 232.08 13145.3 13042.5 -33.7732 8253.05 -30.5562 1414.81 -24.9493 -33.7523 3292.05 -32.5491 -32.0366 231.98 13538.8 13539.5 -34.63 9292.91 -29.1634 1128.88 -17.4044 -34.6222 3022.76 -33.8056 -32.4169 231.88 13633.7 13677.7 -35.5066 9948.59 -26.384 877.514 -3.17962 -35.5038 2735.78 -34.9564 -32.6962 231.78 13211.4 13367.6 -36.3836 10111.7 -21.4331 664.312 21.9193 -36.3826 2441.59 -36.0197 -32.8273 231.68 12500.6 12597 -37.2317 9754.04 -13.1703 489.159 63.7649 -37.2314 2149.55 -36.9932 -32.7476 231.58 10964 11441.1 -38.0275 8936.51 5.65E-04 349.358 129.871 -38.0274 1867.48 -37.8726 -32.3935 231.48 9586 10043.3 -38.7532 7789.85 20.2647 240.695 228.773 -38.7532 1601.51 -38.6536 -31.6996 231.38 8337.95 8575.69 -39.3987 6475.96 50.5352 158.297 368.451 -39.399 1355.99 -39.3354 -30.5991 231.28 7166.94 7197.94 -39.9582 5148.07 94.5882 97.2556 553.535 -39.9592 1133.67 -39.919 -29.0197 231.18 6037.15 6026.05 -40.4393 3923.31 157.146 53.0207 781.382 -40.4425 935.849 -40.4173 -26.8913 231.08 5157.71 5118.76 -40.8518 2872.41 243.904 21.629 1038 -40.8617 762.619 -40.8461 -24.1347 230.98 4741.43 4478.95 -41.1937 2023.21 361.423 -0.20234 1295.84 -41.2227 613.18 -41.2131 -20.6488 230.88 3938.54 4066.88 -41.4595 1371.52 516.798 -15.102 1516.15 -41.5409 486.049 -41.5351 -16.3253 230.78 3940.44 3821.23 -41.6046 893.79 717.103 -25.0912 1657.8 -41.8246 379.313 -41.821 -11.0298 230.68 3422.65 3682.45 -41.5138 557.821 968.478 -31.6847 1690.64 -42.0848 290.81 -42.0827 -4.61014 230.58 3391.52 3611.1 -40.9017 330.473 1274.91 -35.9787 1607.23 -42.3266 218.297 -42.3254 3.11444 230.48 3344 3594.07 -39.144 182.098 1636.65 -38.7571 1425.95 -42.5621 159.556 -42.5614 12.342 230.38 3461.7 3637.73 -34.9109 88.5511 2048.63 -40.5539 1183.46 -42.7937 112.49 -42.7933 23.3067 230.28 3647.8 3753.93 -25.5507 31.4857 2498.82 -41.7355 921.3 -43.0302 75.1695 -43.0299 36.264 230.18 3789.03 3947.65 -6.00549 -2.24492 2967.42 -42.5403 673.995 -43.2752 45.8725 -43.2751 51.5035 230.08 4036.65 4211.94 32.882 -21.6024 3427.04 -43.1217 463.117 -43.5314 23.0929 -43.5313 69.346 229.98 4182.76 4531.13 106.84 -32.4267 3844.57 -43.5787 297.232 -43.803 5.53775 -43.8029 90.1407 229.88 4622.74 4890.12 241.425 -38.3637 4184.82 -43.9717 175.27 -44.0923 -7.88098 -44.0922 114.269 229.78 4986.61 5286.66 475.698 -41.6075 4415.69 -44.3438 90.7074 -44.4075 -18.0708 -44.4074 142.134 229.68 5742.46 5742.89 865.4 -43.4245 4513.65 -44.7198 35.0626 -44.7527 -25.7698 -44.7527 174.172 229.58 6307.48 6312.57 1483.72 -44.5241 4468.28 -45.1188 0.1305 -45.1355 -31.5755 -45.1355 210.838 229.48 7014.29 7079.45 2416.8 -45.2954 4284.36 -45.5602 -20.9042 -45.5686 -35.9689 -45.5686 252.598 229.38 8415.47 8143.07 3750.32 -45.949 3980.91 -46.0633 -33.15 -46.0674 -39.3323 -46.0674 299.933 229.28 9950.74 9589.17 5543.89 -46.5936 3587.43 -46.6414 -40.1392 -46.6434 -41.9602 -46.6434 353.327 229.18 11565.8 11446.1 7793.23 -47.2941 3138.57 -47.3135 -44.1653 -47.3144 -44.0872 -47.3144 413.256 229.08 13479.8 13635.7 10386.9 -48.093 2668.72 -48.1006 -46.6349 -48.101 -45.897 -48.101 480.176 228.98 15737.7 15938.6 13076.2 -49.0115 2207.73 -49.0144 -48.3582 -49.0146 -47.5228 -49.0146 554.518 228.88 18000 18001.4 15485 -50.051 1778.34 -50.0521 -49.7697 -50.0522 -49.0516 -50.0522 636.683 228.78 19314.5 19410 17184.3 -51.1971 1395.44 -51.1975 -51.0806 -51.1975 -50.5324 -51.1975 727.021 228.68 19692.9 19819.7 17822 -52.4113 1066.59 -52.4115 -52.365 -52.4115 -51.9733 -52.4115 825.817 228.58 18659.8 19089.9 17255.7 -53.6392 793.393 -53.6392 -53.6215 -53.6393 -53.3532 -53.6393 933.266 228.48 16771.9 17344.1 15611.7 -54.8173 573.119 -54.8173 -54.8108 -54.8173 -54.6323 -54.8173 1049.44 228.38 14242.2 14919 13232.6 -55.8933 400.317 -55.8933 -55.891 -55.8933 -55.7746 -55.8933 1174.26 228.28 11597 12236.2 10546.9 -56.8279 268.17 -56.8279 -56.8271 -56.8279 -56.7525 -56.8279 1307.44 228.18 9018.73 9670.11 7936.86 -57.6131 169.503 -57.6131 -57.6129 -57.6131 -57.5657 -57.6131 1448.48 228.08 7372.57 7470.75 5660.09 -58.2522 97.4905 -58.2522 -58.2521 -58.2522 -58.2226 -58.2522 1596.64 227.98 5732.65 5750.45 3835.91 -58.7633 46.0632 -58.7633 -58.7633 -58.7633 -58.745 -58.7633 1750.94 227.88 4580.4 4512.63 2474.02 -59.1744 10.0916 -59.1744 -59.1744 -59.1744 -59.1632 -59.1744 1910.15 227.78 4038.21 3694.79 1517.53 -59.5164 -14.5786 -59.5164 -59.5164 -59.5164 -59.5096 -59.5164 2072.79 227.68 3805.44 3207.07 881.469 -59.8083 -31.1804 -59.8083 -59.8083 -59.8083 -59.8042 -59.8083 2237.16 227.58 3583 2958.49 479.186 -60.0688 -42.1595 -60.0688 -60.0688 -60.0688 -60.0664 -60.0688 2401.32 227.48 3360.01 2870.92 236.456 -60.3118 -49.3093 -60.3118 -60.3118 -60.3118 -60.3104 -60.3118 2563.15 227.38 3260.83 2883.96 96.4232 -60.5431 -53.905 -60.5431 -60.5431 -60.5431 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