Figure 3A - XANES Spectra acquired during the synthesis at 270°C. Energy_(eV) Time_(min) Time_label Temperature_(°C) XANES_absorbance_t1_(a.u) XANES_absorbance_t2_(a.u) XANES_absorbance_t3_(a.u) XANES_absorbance_t4_(a.u) XANES_absorbance_t5_(a.u) XANES_absorbance_t6_(a.u) XANES_absorbance_t7_(a.u) XANES_absorbance_t8_(a.u) XANES_absorbance_t9_(a.u) XANES_absorbance_t10_(a.u) XANES_absorbance_t11_(a.u) XANES_absorbance_t12_(a.u) XANES_absorbance_t13_(a.u) XANES_absorbance_t14_(a.u) XANES_absorbance_t15_(a.u) XANES_absorbance_t16_(a.u) XANES_absorbance_t17_(a.u) XANES_absorbance_t18_(a.u) XANES_absorbance_t19_(a.u) XANES_absorbance_t20_(a.u) XANES_absorbance_t21_(a.u) XANES_absorbance_t22_(a.u) XANES_absorbance_t23_(a.u) XANES_absorbance_t24_(a.u) XANES_absorbance_t25_(a.u) XANES_absorbance_t26_(a.u) XANES_absorbance_t27_(a.u) XANES_absorbance_t28_(a.u) XANES_absorbance_t29_(a.u) XANES_absorbance_t30_(a.u) XANES_absorbance_t31_(a.u) XANES_absorbance_t32_(a.u) XANES_absorbance_t33_(a.u) XANES_absorbance_t34_(a.u) XANES_absorbance_t35_(a.u) XANES_absorbance_t36_(a.u) XANES_absorbance_t37_(a.u) XANES_absorbance_t38_(a.u) XANES_absorbance_t39_(a.u) XANES_absorbance_t40_(a.u) XANES_absorbance_t41_(a.u) XANES_absorbance_t42_(a.u) XANES_absorbance_t43_(a.u) 8947.539 0.783333333 t1 25.89607 0.001267935 0.001723457 0.001229541 0.000899690 0.001379397 -0.002236065 0.000154439 0.002009191 0.001416584 0.000470379 0.004547784 0.007328452 0.008336645 0.000933864 0.003397446 0.000393088 0.001526258 0.003510030 0.001673272 0.001970831 0.001536207 -0.000017963 0.000768035 0.003197927 -0.001093385 -0.002839617 -0.002311870 0.003200212 0.000111635 0.005801328 -0.002878763 -0.004360575 0.000896985 0.008269737 0.008475144 -0.001525977 0.001274801 -0.000980873 -0.000128208 0.003734352 -0.004974066 -0.000022265 -0.006736103 8947.910 1.566666667 t2 25.80296 0.001721822 0.001096580 0.001223723 0.000443076 0.000736185 -0.002331257 0.000099020 0.001546445 0.001074632 0.001025144 0.004235616 0.004762850 0.006304026 0.000568296 0.002507307 0.000311047 0.001368421 0.003479921 0.001527529 0.001781788 0.002028593 0.000235201 0.002439085 0.000344428 -0.000223498 -0.000848922 -0.003468189 0.001380024 0.002098196 0.005688729 -0.005016069 -0.004224024 -0.003372242 0.009194940 0.009977787 -0.001145144 -0.000812591 0.000298903 -0.001302883 0.004945664 -0.005198576 0.001184116 -0.005544543 8948.292 2.350000000 t3 25.74885 0.001683110 0.001176978 0.001061239 0.000907225 0.001311935 -0.002043020 -0.000068253 0.001404161 0.001339517 0.001466089 0.001881730 0.004339494 0.006370706 0.000665596 0.002176834 0.000339736 0.000854927 0.002949867 0.000154381 0.001110688 0.000593352 0.000020472 0.001681994 0.001399045 -0.000842194 0.001397609 -0.000396996 0.000277878 0.000247600 0.005664261 -0.002468510 -0.004335985 -0.007443742 0.006160413 0.005509624 -0.000275319 -0.001622619 0.002265255 0.001047347 -0.000161098 -0.005172863 0.043020035 -0.004745484 8948.673 3.133333333 t4 27.46742 0.001319539 0.001105694 0.001103412 0.001532666 0.000985280 -0.000920056 -0.000546500 0.000928781 0.001327778 0.001897661 0.002395546 0.004473264 0.004618919 -0.000129202 0.001616967 0.000492203 0.001488374 0.002645820 0.000934232 0.000488088 0.001670748 -0.000725789 0.005124537 0.001603859 -0.000800951 0.002398598 -0.000146473 0.001209648 0.001584057 0.003934200 -0.002239075 -0.004935671 -0.005630138 0.005787645 0.001936272 0.001368590 -0.001720829 -0.000128014 -0.001803472 0.002591917 -0.002567794 0.003824751 -0.002333608 8949.052 3.916666667 t5 33.66763 0.001265267 0.001262581 0.000977871 0.001354968 0.000533196 -0.001091845 0.000098971 0.001368926 0.000472379 0.002623060 0.002950123 0.002535509 0.004588663 -0.000499028 0.001313245 0.000028143 0.000278542 0.001278276 0.000982259 0.000589467 0.000827433 0.000081872 0.004261715 0.003056378 0.001175138 0.001727168 -0.000178370 -0.001949526 0.002417325 0.002273686 -0.002779662 -0.002324582 -0.002767397 0.005301138 0.002065381 -0.001807850 -0.001303792 -0.001740324 0.001666582 0.002048199 -0.000914354 0.005051966 -0.001830512 8949.464 4.700000000 t6 43.64519 0.000932049 0.000844531 0.001214206 0.000849151 0.001114172 -0.001469544 0.000072338 0.001164594 0.001011701 0.003918654 0.003311531 0.002323631 0.002292962 0.000704576 0.000300909 0.000594258 -0.000513669 0.000659601 0.001074260 0.001160118 0.000033985 0.001004292 0.003164189 0.003119396 0.001576776 0.002086002 0.003029966 -0.000856461 0.002292283 0.003184546 -0.001247242 -0.005030460 -0.000183815 0.001410357 0.002428362 -0.001386473 -0.002195794 0.001728975 0.005426902 0.001087557 -0.002148279 0.000468640 -0.000418826 8949.845 6.266666667 t7 55.77834 0.000161179 0.001037607 0.000632513 0.001335375 0.001094698 -0.000920808 -0.000345990 0.001830672 0.000972527 0.004182780 0.003807216 0.002555274 0.002425190 0.000235568 0.001460854 0.000039130 0.000130351 -0.000846939 0.000709251 0.001015239 0.001057413 0.000401004 0.003380440 0.003964856 0.000747165 0.002840891 0.000897582 0.001622705 -0.000381287 0.002560012 -0.003659529 -0.006360763 0.003049750 0.001117303 -0.003033030 -0.002039725 -0.001519473 -0.001709134 0.005604902 0.002293880 -0.002963262 -0.000388167 -0.002202250 8950.246 7.050000000 t8 67.13223 0.000697862 0.001351834 0.000268052 0.000981345 0.001327249 -0.000900362 -0.000563569 0.001437720 0.000857294 0.004636900 0.002381990 0.002492840 0.003954937 0.000224571 0.000205822 0.000422838 0.000134964 -0.001240189 0.001051705 0.000701962 0.000263011 0.000866109 0.004981018 0.002114317 0.003039640 0.004848849 0.000872069 0.003033339 0.000706817 0.000646587 -0.004125801 -0.003617345 0.002268730 0.000163694 -0.002128217 -0.000909919 0.001157341 0.003356784 0.008784662 0.001874416 -0.003289457 -0.001323063 0.001692356 8950.653 7.833333333 t9 78.67744 0.000533223 0.001261387 0.001440217 0.000919550 0.000485055 -0.000138996 -0.000326481 0.001574106 0.001027039 0.003445755 0.001541900 0.000912566 0.004987101 0.000865815 -0.000203318 -0.000085386 0.000020138 -0.001660454 0.001557211 0.001159288 -0.000092854 -0.000164161 0.004084801 0.002272937 0.001198585 0.002673680 0.002126855 0.003777790 -0.001554556 -0.003389783 -0.003480257 -0.001137480 0.005557715 -0.001565021 -0.005419340 -0.000779369 0.002862916 0.003491736 0.006996460 0.001633657 -0.000997665 0.000584871 0.000628384 8951.051 8.616666667 t10 89.15585 0.000039496 -0.000154422 0.000770440 0.000789511 0.000133651 0.000087859 -0.000662650 0.001245622 0.000392997 0.003234840 -0.000374112 -0.000490452 0.005530620 -0.000440142 0.000756218 0.001326027 -0.000224576 0.001042265 -0.000661736 0.000330833 0.000391599 0.000955376 0.004291763 0.001206520 0.001887344 0.001734321 0.002167409 -0.000885679 0.000917445 -0.002672951 -0.002729725 -0.002438947 0.003147229 -0.003071306 -0.005710386 -0.000604847 0.006171577 0.005079011 0.005758086 -0.000659118 0.001867605 0.008142265 0.002376992 8951.467 9.400000000 t11 98.85664 0.000016300 0.000699471 0.000236092 0.000448041 0.000558538 -0.000164705 -0.000023484 0.001029372 0.000498564 0.003899146 -0.001312405 0.000206348 0.004624352 0.000450657 0.000172076 0.000022214 -0.000659125 0.000340665 -0.000836893 0.000179716 -0.000676706 0.001042461 0.003946107 -0.000893232 0.000131150 0.001793387 0.001530251 0.001189222 -0.002068931 -0.002053991 -0.000825609 -0.005805534 0.005943274 -0.002479957 -0.003764581 0.002772621 0.003217191 0.004579857 0.001644074 -0.000088114 -0.001782088 0.001770624 0.003671937 8951.866 10.183333333 t12 106.91299 -0.000389697 0.000420526 0.000927202 -0.000297702 0.000236132 -0.000230325 0.000066564 0.001302597 0.000662076 0.003532834 -0.002167013 0.000341231 0.003885367 0.000265956 -0.001245019 0.000141232 -0.000418694 0.000840077 -0.002453512 0.000294351 -0.000393421 0.001180420 0.003918343 0.000584016 -0.000809775 -0.001505785 0.001792363 0.000859158 -0.001394413 -0.002405153 -0.001527489 -0.005838570 0.002118595 -0.000800938 -0.005569582 0.004270541 0.006454011 0.001988937 0.000561783 -0.000073587 0.002256581 0.010616579 0.001278709 8952.271 10.966666667 t13 119.12085 -0.000090829 0.000421675 0.000259446 0.000271076 0.000206113 0.000994214 0.000301098 0.000188308 0.000267088 0.002977984 -0.003698606 0.000407425 0.003307501 0.001009257 -0.001382257 -0.000125995 0.000073716 0.000919873 -0.000219417 0.000818495 -0.000226414 0.000396132 0.003898238 0.002486475 0.001074044 0.000845928 0.000707329 -0.002110965 -0.000634604 -0.001659756 -0.004076999 -0.003707618 0.000472086 -0.001220657 -0.003822631 -0.000637917 0.001380237 -0.001264384 -0.000181129 0.000380158 0.002538187 -0.002592296 0.000263997 8952.677 11.750000000 t14 135.56233 -0.000102349 0.000223390 -0.000064363 0.000069330 0.000372947 0.000687463 0.000440744 -0.000244198 0.001150154 0.002260928 -0.002884164 -0.000121148 0.000729961 0.000651111 -0.000353769 0.000259741 -0.001788618 -0.000283454 -0.000006139 -0.000277469 0.000263531 0.000017531 0.004335158 0.002656558 0.001023077 -0.001946082 0.000807589 -0.002209562 0.000879486 -0.003216385 -0.003696053 -0.004774882 0.001123919 -0.000951829 -0.001043377 -0.001777644 -0.000716556 -0.001097503 -0.001228842 0.001250446 0.001231649 -0.001481756 0.003832874 8953.088 12.533333333 t15 153.7296 -0.000263016 -0.000010267 0.000940492 0.000019419 0.000377165 0.000916384 0.000713352 -0.000476543 0.001115808 0.001244499 -0.002447985 0.001876141 -0.000345163 0.000447006 -0.000760413 0.000159696 -0.000439037 -0.000037422 -0.000034757 -0.000619771 0.000181425 0.000938144 0.002302261 0.001179621 0.001923380 0.000790420 0.002087757 -0.001527714 0.002073739 -0.001409435 -0.002098729 -0.004991928 0.002236818 -0.001718354 -0.001867163 -0.002995822 0.002028162 -0.002341126 -0.003138312 -0.001076393 0.001509668 -0.003822516 0.007470125 8953.470 13.316666667 t16 169.8987 -0.000009269 -0.000076158 -0.000196580 -0.000002673 0.000096462 0.000865572 0.000651577 -0.000101399 0.000430974 -0.000755446 -0.002235061 0.002886732 -0.004654823 0.000416766 -0.000197821 0.000841538 -0.000278118 -0.000437393 0.000019882 0.000000294 -0.001132974 0.001527821 -0.002015714 0.000126578 0.003011350 0.000714704 0.001988792 -0.000542990 0.001498664 -0.002167211 -0.002208937 -0.003565835 0.001403149 -0.002443613 -0.000115432 -0.004275607 -0.001885110 -0.003040943 -0.004413124 -0.000890006 0.002774307 -0.000831239 0.005444403 8953.883 14.100000000 t17 184.37155 0.000086205 -0.000463718 0.000062098 -0.000458221 0.000173143 0.001884570 0.000603049 -0.000698161 -0.000111673 -0.001980806 -0.001265378 0.002693442 -0.008118934 0.001325168 0.000102740 0.001082125 -0.000553521 -0.000382991 -0.000283298 -0.001371630 -0.002016733 0.003331820 -0.004554839 0.001754466 0.002006180 0.000244076 0.002097971 -0.000118051 0.002901735 -0.002007896 -0.002835450 -0.000985825 -0.000956715 -0.004839572 0.002031424 -0.003723430 -0.002242414 -0.004633695 -0.002928796 0.001259994 -0.001306430 -0.003439822 0.004974681 8954.293 14.883333333 t18 197.56111 -0.000244879 -0.000235352 0.000040993 -0.000746270 -0.000398573 0.001156508 0.000843481 -0.000229054 -0.000524870 -0.003852250 0.000166106 0.001642933 -0.008516638 -0.000052271 -0.000600900 0.000658110 0.000170438 -0.000578184 -0.000007828 -0.000052488 -0.003361442 0.001436250 -0.005639770 0.002525442 0.002776599 0.000369409 -0.000478910 0.001476447 0.004987813 -0.002748003 -0.004012626 0.001493525 0.001618233 -0.005631837 0.000903261 -0.002868992 0.000438368 -0.000854230 -0.000311992 -0.000338705 0.003039493 -0.006704800 0.006272141 8954.702 15.666666667 t19 208.93806 0.000085527 -0.000492723 -0.000343502 -0.000199631 -0.000084977 0.001184613 0.000871415 -0.001046109 -0.000557991 -0.003546420 0.002087488 -0.001678636 -0.005814403 0.000064921 -0.000675756 0.001171195 0.000236613 -0.001032630 0.000470115 -0.001034077 -0.002308103 -0.000192111 -0.004710447 0.000999865 0.002370426 0.001983122 0.002041598 0.000973079 0.000562501 -0.002042701 -0.005095688 0.002514413 0.001860340 -0.001956792 -0.000034490 -0.000515655 0.001341992 0.001703409 0.002339945 0.002724257 0.002581737 -0.002878842 0.003477104 8955.108 16.450000000 t20 220.03418 -0.000522767 -0.000921818 -0.000519295 -0.000174191 -0.000335002 0.001033196 0.001055335 -0.000969696 -0.001152872 -0.004469538 0.004863246 -0.002302403 -0.002826806 -0.000216373 -0.001706969 0.000820401 0.000098831 -0.000462433 0.000940619 -0.000661348 -0.001436994 -0.000923360 -0.004728748 0.002154473 0.000955486 0.000494874 0.001586314 -0.000094013 0.003119360 -0.000522427 -0.002312593 0.005280970 0.003304872 -0.003254564 -0.000150247 0.002090902 0.003038496 0.001300462 -0.001012218 0.002767177 -0.002021482 -0.003706806 0.003690154 8955.487 17.233333333 t21 229.60359 -0.000679018 -0.000855652 -0.000461130 -0.000092120 -0.001193305 0.001345438 0.000834663 -0.001349701 -0.001659551 -0.004660318 0.007241470 0.001427009 -0.000905665 -0.000795744 -0.002268089 0.000468260 0.001001547 -0.000475234 0.000646922 -0.000685839 -0.003624151 0.004565825 -0.005896963 0.002363007 -0.004089966 0.000376047 -0.000397955 -0.001654209 0.004752532 -0.001598009 -0.001049421 0.004955587 0.003288867 -0.006941570 -0.000075119 0.001926255 0.002586632 0.000239171 -0.000560750 -0.000137091 -0.000009591 -0.005186582 0.001854172 8955.898 18.800000000 t22 230.93825 -0.000276660 -0.000598807 -0.001557394 -0.000445587 -0.000597592 0.001367308 0.000221635 -0.001275975 -0.001253703 -0.005271563 0.007559963 0.002528944 0.000441520 -0.000297095 -0.001404251 0.000078479 0.000666636 -0.000680193 0.000239724 0.000481874 -0.000566482 0.004281580 -0.005208458 -0.000790071 -0.007271416 -0.001803478 -0.001638726 -0.001314842 0.003144564 -0.004719522 0.002226764 0.007460790 0.002288229 -0.002231641 0.000701495 0.003017091 0.002518733 -0.002729994 0.000886288 0.003274518 0.005581695 -0.004894352 -0.000699459 8956.287 19.583333333 t23 252.23669 -0.000891179 -0.000568088 -0.001278975 -0.000695709 -0.000328417 0.001770182 0.000463993 -0.001166942 -0.001456135 -0.006163666 0.008986545 0.002696080 0.002400278 -0.000162083 -0.001231245 0.000722443 0.000010151 -0.000590341 -0.000348976 0.001369899 -0.001462592 0.003162757 -0.004680909 -0.001578066 -0.006492604 -0.002901042 -0.001363971 -0.002318302 0.002343765 -0.002531623 0.002358559 0.004804757 0.001647119 -0.002150701 -0.000304920 -0.003821950 0.001448314 -0.000934113 -0.003772106 -0.002448441 0.004652141 -0.004352663 0.003383448 8956.696 20.366666667 t24 258.40253 -0.000507450 -0.000980978 -0.000692180 -0.000852731 -0.001090428 0.001049994 0.000357204 -0.001017100 -0.000977039 -0.005780287 0.009041325 0.001462169 0.001950645 -0.001353769 0.000096747 -0.000094264 0.000685063 -0.000736616 -0.000458380 0.000610658 -0.001221779 0.001304513 -0.002851679 -0.001424573 -0.002604940 -0.006181674 0.000292176 -0.000561690 0.001162003 -0.001548348 0.004143148 0.004399427 0.001317988 0.000399220 0.000334344 -0.003406427 -0.000381985 -0.001621373 -0.002265380 -0.003871632 0.004560615 -0.003720106 0.002621147 8957.075 21.150000000 t25 264.23196 -0.001193406 -0.000669986 -0.000670097 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