August 6, 2020 Journal article Open Access

Dzmitry V. Yakimchuk; Victoria D. Bundyukova; Jon Ustarroz; Herman Terryn; Kitty Baert; Artem L. Kozlovskiy; Maxim V. Zdorovets; Soslan A. Khubezhov; Alex V. Trukhanov; Sergei V. Trukhanov; Larissa V. Panina; Grigory M. Arzumanyan; Kahramon Z. Mamatkulov; Daria I. Tishkevich; Egor Y. Kaniukov; Vladimir Sivakov

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  <identifier identifierType="URL">https://zenodo.org/record/3993464</identifier>
  <creators>
    <creator>
      <creatorName>Dzmitry V. Yakimchuk</creatorName>
      <affiliation>Cryogenic Research Division, Scientific-Practical Materials Research Centre, NAS of Belarus, 220072 Minsk, Belarus</affiliation>
    </creator>
    <creator>
      <creatorName>Victoria D. Bundyukova</creatorName>
      <affiliation>Cryogenic Research Division, Scientific-Practical Materials Research Centre, NAS of Belarus, 220072 Minsk, Belarus</affiliation>
    </creator>
    <creator>
      <creatorName>Jon Ustarroz</creatorName>
      <affiliation>Department Materials and Chemistry, Vrije Universiteit Brussel, Boulevard de la Plaine 5, 1050 Brussels, Belgium &amp; ChemSIN—Chemstry of Surfaces, Interfaces and Nanomaterials, Université libre de Bruxcelles, Campus de la Plaine, Boulevard du Triomphe 2, CP 255. 1050 Brussels, Belgium</affiliation>
    </creator>
    <creator>
      <creatorName>Herman Terryn</creatorName>
      <affiliation>Department Materials and Chemistry, Vrije Universiteit Brussel, Boulevard de la Plaine 5, 1050 Brussels, Belgium</affiliation>
    </creator>
    <creator>
      <creatorName>Kitty Baert</creatorName>
      <affiliation>Department Materials and Chemistry, Vrije Universiteit Brussel, Boulevard de la Plaine 5, 1050 Brussels, Belgium</affiliation>
    </creator>
    <creator>
      <creatorName>Artem L. Kozlovskiy</creatorName>
      <affiliation>Laboratory of Solid State Physics, The Institute of Nuclear Physics, Ibragimov Str. 1, Nur-Sultan 050032, Kazakhstan &amp; Laboratory of Engineering Profile, L.N. Gumilyov Eurasian National University, Mirzoyan Str. 2, Nur-Sultan 010008, Kazakhstan</affiliation>
    </creator>
    <creator>
      <creatorName>Maxim V. Zdorovets</creatorName>
      <affiliation>Laboratory of Solid State Physics, The Institute of Nuclear Physics, Ibragimov Str. 1, Nur-Sultan 050032, Kazakhstan &amp; Laboratory of Engineering Profile, L.N. Gumilyov Eurasian National University, Mirzoyan Str. 2, Nur-Sultan 010008, Kazakhstan &amp; Department of Intelligent Information Technologies, Ural Federal University, Prospekt Lenina 51, 620002 Yekaterinburg, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Soslan A. Khubezhov</creatorName>
      <affiliation>Department of Physics, North-Ossetian State University, Vatutina Str. 46, 362025 Vladikavkaz, Russia &amp; Department of Physics and Engineering, ITMO University, Kronverkskiy Prospekt, St. 197101 Petersburg, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Alex V. Trukhanov</creatorName>
      <affiliation>Cryogenic Research Division, Scientific-Practical Materials Research Centre, NAS of Belarus, 220072 Minsk, Belarus &amp; Laboratory of Single Crystal Growth, South Ural State University, Lenin prospekt, Chelyabinsk 76, 454080 Chelyabinsk, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Sergei V. Trukhanov</creatorName>
      <affiliation>Cryogenic Research Division, Scientific-Practical Materials Research Centre, NAS of Belarus, 220072 Minsk, Belarus &amp; Laboratory of Single Crystal Growth, South Ural State University, Lenin prospekt, Chelyabinsk 76, 454080 Chelyabinsk, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Larissa V. Panina</creatorName>
      <affiliation>Department of Electronic Materials Technology, National University of Science and Technology MISiS, 119049 Moscow, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Grigory M. Arzumanyan</creatorName>
      <affiliation>Department of Raman Spectroscopy (Centre "Nanobiophotonics"), Joint Institute for Nuclear Research, 6 St. Joliot-Curie, 141980 Dubna, Russia &amp; Faculty of Nanotechnologies and New Materials, Dubna State University, Ulitsa Universitetskaya, 19, 141982 Dubna, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Kahramon Z. Mamatkulov</creatorName>
      <affiliation>Department of Raman Spectroscopy (Centre "Nanobiophotonics"), Joint Institute for Nuclear Research, 6 St. Joliot-Curie, 141980 Dubna, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Daria I. Tishkevich</creatorName>
      <affiliation>Cryogenic Research Division, Scientific-Practical Materials Research Centre, NAS of Belarus, 220072 Minsk, Belarus &amp; Laboratory of Single Crystal Growth, South Ural State University, Lenin prospekt, Chelyabinsk 76, 454080 Chelyabinsk, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Egor Y. Kaniukov</creatorName>
      <affiliation>Laboratory of Single Crystal Growth, South Ural State University, Lenin prospekt, Chelyabinsk 76, 454080 Chelyabinsk, Russia &amp; Department of Electronic Materials Technology, National University of Science and Technology MISiS, 119049 Moscow, Russia</affiliation>
    </creator>
    <creator>
      <creatorName>Vladimir Sivakov</creatorName>
      <nameIdentifier nameIdentifierScheme="ORCID" schemeURI="http://orcid.org/">0000-0002-3272-501X</nameIdentifier>
      <affiliation>Departament of Functional Interfaces, Leibniz Institute of Photonic Technology, Albert-Einstein-Str. 9, 07745 Jena, Germany</affiliation>
    </creator>
  </creators>
  <titles>
    <title>Morphology and Microstructure Evolution of Gold Nanostructures in the Limited Volume Porous Matrices</title>
  </titles>
  <publisher>Zenodo</publisher>
  <publicationYear>2020</publicationYear>
  <subjects>
    <subject>gold</subject>
    <subject>nanostructures</subject>
    <subject>template synthesis</subject>
    <subject>X-ray diffraction</subject>
    <subject>X-ray photoelectron spectroscopy</subject>
    <subject>growth mechanism</subject>
    <subject>SERS</subject>
  </subjects>
  <dates>
    <date dateType="Issued">2020-08-06</date>
  </dates>
  <language>en</language>
  <resourceType resourceTypeGeneral="JournalArticle"/>
  <alternateIdentifiers>
    <alternateIdentifier alternateIdentifierType="url">https://zenodo.org/record/3993464</alternateIdentifier>
  </alternateIdentifiers>
  <relatedIdentifiers>
    <relatedIdentifier relatedIdentifierType="DOI" relationType="IsIdenticalTo">10.3390/s20164397</relatedIdentifier>
  </relatedIdentifiers>
  <rightsList>
    <rights rightsURI="https://creativecommons.org/licenses/by/4.0/legalcode">Creative Commons Attribution 4.0 International</rights>
    <rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights>
  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">&lt;p&gt;The modern development of nanotechnology requires the discovery of simple approaches that ensure the controlled formation of functional nanostructures with a predetermined morphology. One of the simplest approaches is the self-assembly of nanostructures. The widespread implementation of self-assembly is limited by the complexity of controlled processes in a large volume where, due to the temperature, ion concentration, and other thermodynamics factors, local changes in diffusion-limited processes may occur, leading to unexpected nanostructure growth. The easiest ways to control the diffusion-limited processes are spatial limitation and localized growth of nanostructures in a porous matrix. In this paper, we propose to apply the method of controlled self-assembly of gold nanostructures in a limited pore volume of a silicon oxide matrix with submicron pore sizes. A detailed study of achieved gold nanostructures&amp;rsquo; morphology, microstructure, and surface composition at different formation stages is carried out to understand the peculiarities of realized nanostructures. Based on the obtained results, a mechanism for the growth of gold nanostructures in a limited volume, which can be used for the controlled formation of nanostructures with a predetermined geometry and composition, has been proposed. The results observed in the present study can be useful for the design of plasmonic-active surfaces for surface-enhanced Raman spectroscopy-based detection of ultra-low concentration of different chemical or biological analytes, where the size of the localized gold nanostructures is comparable with the spot area of the focused laser beam.&lt;/p&gt;</description>
  </descriptions>
  <fundingReferences>
    <fundingReference>
      <funderName>European Commission</funderName>
      <funderIdentifier funderIdentifierType="Crossref Funder ID">10.13039/100010661</funderIdentifier>
      <awardNumber awardURI="info:eu-repo/grantAgreement/EC/H2020/778308/">778308</awardNumber>
      <awardTitle>Physical principles of the creation of novel SPINtronic materials on the
base of MULTIlayered metal-oxide FILMs for magnetic sensors and MRAM</awardTitle>
    </fundingReference>
  </fundingReferences>
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