April 30, 2020 Journal article Open Access

Nikolay Kalanda; Marta Yarmolich; Maksim Kutuzau; Alexander Gurskii; Maria do RosárioTeixeira Soares; Mindaugas Andrulevičius; Brigita Abakevičienė; Sigitas Tamulevičius

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    <subfield code="a">&lt;p&gt;The sequence of phase transformations during the crystallization of SrBaFeMoO&lt;sub&gt;6&amp;ndash;&amp;delta; &lt;/sub&gt;by the solid-phase technique from a stoichiometric mixture of simple oxides SrCO&lt;sub&gt;3&lt;/sub&gt; + BaCO&lt;sub&gt;3&lt;/sub&gt; + 0.5Fe&lt;sub&gt;2&lt;/sub&gt;O&lt;sub&gt;3&lt;/sub&gt; + MoO&lt;sub&gt;3&lt;/sub&gt;was studied. It has been established that the synthesis of barium &amp;ndash; strontium ferromolybdate proceeds through a series of sequential - parallel stages. It was found that to minimize the effect of intermediate reaction products, it is necessary to use combined synthesis modes. As a result of using combined synthesis modes for annealing for 20 hours and T = 1443 K in vacuum of 10&lt;sup&gt;-5&lt;/sup&gt;Torr at the pressure of residual oxygen gas 10&lt;sup&gt;-8 &lt;/sup&gt;Pa, it was possible to obtain a single-phase barium &amp;ndash; strontium ferromolybdate compound with superstructural ordering of iron and molybdenum cations.&lt;/p&gt;</subfield>
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