Dataset Open Access

Raw Data of Pilot Plant Runs for CONSENS Project (Case Study 1)

Simon Kern; Lukas Wander; Klas Meyer; Svetlana Guhl; Anwesh Reddy Gottu Mukkula; Manuel Holtkamp; Malte Salge; Christoph Fleischer; Nils Weber; Rudibert King; Sebastian Engell; Andrea Paul; Manuel Pereira Remelhe; Michael Maiwald


Citation Style Language JSON Export

{
  "publisher": "Zenodo", 
  "DOI": "10.5281/zenodo.1438233", 
  "language": "eng", 
  "title": "Raw Data of Pilot Plant Runs for CONSENS Project (Case Study 1)", 
  "issued": {
    "date-parts": [
      [
        2018, 
        9, 
        28
      ]
    ]
  }, 
  "abstract": "<p>In&nbsp;case study one of the CONSENS project, two aromatic substances were coupled by a lithiation reaction, which is a prominent example in pharmaceutical industry. The two aromatic reactants (Aniline and <em>o</em>-FNB) were mixed with Lithium-base (LiHMDS)&nbsp;in a continuous modular plant&nbsp;to produce the desired product (Li-NDPA) and a salt (LiF). The salt precipitates which leads to the formation of particles. The feed streams were&nbsp;subject to&nbsp;variation to drive the plant to its optimum.&nbsp;</p>\n\n<p>The uploaded data comprises the results from four days during continuous plant operation time. Each day is denoted from day 1-4 and represents the dates 2017-09-26,&nbsp;2017-09-28,&nbsp;2017-10-10,&nbsp;2017-10-17.</p>\n\n<p>In the following the contents of the files are explained.</p>\n\n<p><strong>NIR_data_AQ15_raw.zip: </strong>Contains Bruker binary files (0-Files)&nbsp;of NIR spectrometer at AQ15 (Location is located subsequently to NMR spectrometer)</p>\n\n<p><strong>NMR_spectra_raw.zip:&nbsp;</strong>Contains Spinsolve files (Binarys of&nbsp;FID and Spectrum, DX-Files) of NMR spectrometer. The use of DX-files files is not recommended.</p>\n\n<p><strong>PCS_data_csv.zip</strong>: Contains csv-files of the process control system (PCS) including data of mass flow controlers (*_Bilanz.csv),&nbsp;filling level (*_FillLe.csv), pressures (*_pres), temperatures (*_Temp), position of valves (*_Valves). Relevant labels are: BP13 = LiHMDS&nbsp;storage tank, BP12 = aniline storage tank, BP12 = <em>o</em>-FNB storage tank, CM003 and CM004 = tubular reactors, T0041 and T005 = Temperature at reactor exits, P009 and P003 = Pressure at reactor inlets, P006 = Pressure at reactor exits.</p>\n\n<p><strong>housing_data_NMR.csv</strong>: Contrains data of NMR enclosure of all four days. Each columns from left to right represent timestamps, bypass pressure (bar), bypass temperature (&deg;C), Gasalarm (logical), bypass actual flowrate (g&nbsp;min<sup>-1</sup>),&nbsp; bypass flowrate setpoint (g&nbsp;min<sup>-1</sup>), bypass density (kg&nbsp;m<sup>3</sup>)</p>\n\n<p><strong>matlab_variables_explanation.xlsx</strong>: Explanation of variables used in matlab structure &quot;data_validation_run&quot;.</p>\n\n<p><strong>data_validation_run.mat</strong>: Matlab structure containing most relevant process data including NMR results, NIR results, housing data of NMR, and process control system data.</p>", 
  "author": [
    {
      "family": "Simon Kern"
    }, 
    {
      "family": "Lukas Wander"
    }, 
    {
      "family": "Klas Meyer"
    }, 
    {
      "family": "Svetlana Guhl"
    }, 
    {
      "family": "Anwesh Reddy Gottu Mukkula"
    }, 
    {
      "family": "Manuel Holtkamp"
    }, 
    {
      "family": "Malte Salge"
    }, 
    {
      "family": "Christoph Fleischer"
    }, 
    {
      "family": "Nils Weber"
    }, 
    {
      "family": "Rudibert King"
    }, 
    {
      "family": "Sebastian Engell"
    }, 
    {
      "family": "Andrea Paul"
    }, 
    {
      "family": "Manuel Pereira Remelhe"
    }, 
    {
      "family": "Michael Maiwald"
    }
  ], 
  "version": "1.0", 
  "type": "dataset", 
  "id": "1438233"
}
134
41
views
downloads
All versions This version
Views 134134
Downloads 4141
Data volume 59.0 GB59.0 GB
Unique views 103103
Unique downloads 1717

Share

Cite as