Dataset Open Access

Br soaked lysozyme datasets collected with the mixed scheme implemented in HITO in the ZOO system

Kunio Hirata


MARC21 XML Export

<?xml version='1.0' encoding='UTF-8'?>
<record xmlns="http://www.loc.gov/MARC21/slim">
  <leader>00000nmm##2200000uu#4500</leader>
  <controlfield tag="005">20190107133235.0</controlfield>
  <controlfield tag="001">1208078</controlfield>
  <datafield tag="856" ind1="4" ind2=" ">
    <subfield code="s">40654331336</subfield>
    <subfield code="z">md5:d237f22cd25fe3ca8723c670394ee1a3</subfield>
    <subfield code="u">https://zenodo.org/record/1208078/files/hito-CPS1991-05.tgz</subfield>
  </datafield>
  <datafield tag="542" ind1=" " ind2=" ">
    <subfield code="l">open</subfield>
  </datafield>
  <datafield tag="260" ind1=" " ind2=" ">
    <subfield code="c">2018-12-18</subfield>
  </datafield>
  <datafield tag="909" ind1="C" ind2="O">
    <subfield code="p">openaire_data</subfield>
    <subfield code="p">user-zenodo</subfield>
    <subfield code="o">oai:zenodo.org:1208078</subfield>
  </datafield>
  <datafield tag="100" ind1=" " ind2=" ">
    <subfield code="u">RIKEN/SPring-8 Center</subfield>
    <subfield code="0">(orcid)0000-0002-1491-6509</subfield>
    <subfield code="a">Kunio Hirata</subfield>
  </datafield>
  <datafield tag="245" ind1=" " ind2=" ">
    <subfield code="a">Br soaked lysozyme datasets collected with the mixed scheme implemented in HITO in the ZOO system</subfield>
  </datafield>
  <datafield tag="980" ind1=" " ind2=" ">
    <subfield code="a">user-zenodo</subfield>
  </datafield>
  <datafield tag="540" ind1=" " ind2=" ">
    <subfield code="u">http://creativecommons.org/licenses/by/4.0/legalcode</subfield>
    <subfield code="a">Creative Commons Attribution 4.0 International</subfield>
  </datafield>
  <datafield tag="650" ind1="1" ind2="7">
    <subfield code="a">cc-by</subfield>
    <subfield code="2">opendefinition.org</subfield>
  </datafield>
  <datafield tag="520" ind1=" " ind2=" ">
    <subfield code="a">&lt;p&gt;Bromide soaked lysozyme crystals were used as standard crystals for evaluation of the automated data collection, ZOO, developed at SPring-8 BL32XU.&lt;/p&gt;

&lt;p&gt;Crystals those sizes ranged 10-100 &amp;micro;m were cryocooled together in the same cryoloop and processed &amp;#39;mixed scheme&amp;#39; implemented in the ZOO system.&lt;/p&gt;

&lt;p&gt;Beam size : 10(H) x 15(V) &amp;micro;m&lt;sup&gt;2&lt;/sup&gt;&lt;/p&gt;

&lt;p&gt;After 2D raster scanning the loop, HITO detects 1&amp;nbsp;crystals for full rotation helical, 7 crystals for partial helical, and 62 crystals for multiple small wedge schemes, respectively. A full rotation helical, partial helical and small wedge datasets contain total oscillation of 60 deg, 40 deg and 5 deg. respectively.&amp;nbsp;&lt;/p&gt;

&lt;p&gt;The crystals belong&amp;nbsp;to space group P4&lt;sub&gt;3&lt;/sub&gt;2&lt;sub&gt;1&lt;/sub&gt;2 with mean unit cell parameters a=b=79.1, c=37.5.&lt;/p&gt;

&lt;p&gt;Data was processed up to&amp;nbsp;1.50 &amp;Aring; resolution in the published result (Hirata et al. in preparation) using KAMO.&lt;/p&gt;

&lt;p&gt;&lt;em&gt;&lt;strong&gt;&amp;lt;Available data&amp;gt;&lt;/strong&gt;&lt;/em&gt;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;# Beamline: &amp;nbsp; &amp;nbsp; SPring-8 BL32XU&lt;/li&gt;
	&lt;li&gt;# wavelength&amp;nbsp; &amp;nbsp; 0.9000 A&lt;/li&gt;
	&lt;li&gt;# Detector :&amp;nbsp; &amp;nbsp; EIGER X 9M&lt;/li&gt;
	&lt;li&gt;# ZOO mode: mixed scheme (HITO)&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# Multiple small wedge datasets&lt;/li&gt;
	&lt;li&gt;# &amp;#39;CPS1991-05-multi_master.h5&amp;#39; manages 62 datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 5.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;# 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 50 frames / datasets&lt;/li&gt;
	&lt;li&gt;# 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000005.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000006.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000007.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000008.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000009.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000010.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000011.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000012.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000013.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000014.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000015.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000016.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000017.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000018.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000019.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000020.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000021.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000022.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000023.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000024.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000025.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000026.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000027.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000028.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000029.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000030.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000031.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_master.h5&lt;/li&gt;
&lt;/ul&gt;

&lt;p&gt;&amp;nbsp;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# &amp;#39;cry-00-??_master.h5&amp;#39; are for &amp;#39;partial helical&amp;#39; datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 40.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 400 frames / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_master.h5&lt;/li&gt;
&lt;/ul&gt;

&lt;p&gt;&amp;nbsp;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# &amp;#39;cry-01-??_master.h5&amp;#39; are for &amp;#39;full rotation helical&amp;#39; datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 60.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 600 frames / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;# ** The program could collect &amp;#39;full rotation&amp;#39; helical dataset&lt;/li&gt;
	&lt;li&gt;# but 60 deg. was set for this demonstration.&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000005.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000006.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_master.h5&lt;/li&gt;
&lt;/ul&gt;</subfield>
  </datafield>
  <datafield tag="773" ind1=" " ind2=" ">
    <subfield code="n">doi</subfield>
    <subfield code="i">isVersionOf</subfield>
    <subfield code="a">10.5281/zenodo.1208077</subfield>
  </datafield>
  <datafield tag="024" ind1=" " ind2=" ">
    <subfield code="a">10.5281/zenodo.1208078</subfield>
    <subfield code="2">doi</subfield>
  </datafield>
  <datafield tag="980" ind1=" " ind2=" ">
    <subfield code="a">dataset</subfield>
  </datafield>
</record>
181
7
views
downloads
All versions This version
Views 181181
Downloads 77
Data volume 284.6 GB284.6 GB
Unique views 142142
Unique downloads 77

Share

Cite as