Dataset Open Access

Br soaked lysozyme datasets collected with the mixed scheme implemented in HITO in the ZOO system

Kunio Hirata


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  <identifier identifierType="DOI">10.5281/zenodo.1208078</identifier>
  <creators>
    <creator>
      <creatorName>Kunio Hirata</creatorName>
      <nameIdentifier nameIdentifierScheme="ORCID" schemeURI="http://orcid.org/">0000-0002-1491-6509</nameIdentifier>
      <affiliation>RIKEN/SPring-8 Center</affiliation>
    </creator>
  </creators>
  <titles>
    <title>Br soaked lysozyme datasets collected with the mixed scheme implemented in HITO in the ZOO system</title>
  </titles>
  <publisher>Zenodo</publisher>
  <publicationYear>2018</publicationYear>
  <dates>
    <date dateType="Issued">2018-12-18</date>
  </dates>
  <resourceType resourceTypeGeneral="Dataset"/>
  <alternateIdentifiers>
    <alternateIdentifier alternateIdentifierType="url">https://zenodo.org/record/1208078</alternateIdentifier>
  </alternateIdentifiers>
  <relatedIdentifiers>
    <relatedIdentifier relatedIdentifierType="DOI" relationType="IsVersionOf">10.5281/zenodo.1208077</relatedIdentifier>
    <relatedIdentifier relatedIdentifierType="URL" relationType="IsPartOf">https://zenodo.org/communities/zenodo</relatedIdentifier>
  </relatedIdentifiers>
  <rightsList>
    <rights rightsURI="http://creativecommons.org/licenses/by/4.0/legalcode">Creative Commons Attribution 4.0 International</rights>
    <rights rightsURI="info:eu-repo/semantics/openAccess">Open Access</rights>
  </rightsList>
  <descriptions>
    <description descriptionType="Abstract">&lt;p&gt;Bromide soaked lysozyme crystals were used as standard crystals for evaluation of the automated data collection, ZOO, developed at SPring-8 BL32XU.&lt;/p&gt;

&lt;p&gt;Crystals those sizes ranged 10-100 &amp;micro;m were cryocooled together in the same cryoloop and processed &amp;#39;mixed scheme&amp;#39; implemented in the ZOO system.&lt;/p&gt;

&lt;p&gt;Beam size : 10(H) x 15(V) &amp;micro;m&lt;sup&gt;2&lt;/sup&gt;&lt;/p&gt;

&lt;p&gt;After 2D raster scanning the loop, HITO detects 1&amp;nbsp;crystals for full rotation helical, 7 crystals for partial helical, and 62 crystals for multiple small wedge schemes, respectively. A full rotation helical, partial helical and small wedge datasets contain total oscillation of 60 deg, 40 deg and 5 deg. respectively.&amp;nbsp;&lt;/p&gt;

&lt;p&gt;The crystals belong&amp;nbsp;to space group P4&lt;sub&gt;3&lt;/sub&gt;2&lt;sub&gt;1&lt;/sub&gt;2 with mean unit cell parameters a=b=79.1, c=37.5.&lt;/p&gt;

&lt;p&gt;Data was processed up to&amp;nbsp;1.50 &amp;Aring; resolution in the published result (Hirata et al. in preparation) using KAMO.&lt;/p&gt;

&lt;p&gt;&lt;em&gt;&lt;strong&gt;&amp;lt;Available data&amp;gt;&lt;/strong&gt;&lt;/em&gt;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;# Beamline: &amp;nbsp; &amp;nbsp; SPring-8 BL32XU&lt;/li&gt;
	&lt;li&gt;# wavelength&amp;nbsp; &amp;nbsp; 0.9000 A&lt;/li&gt;
	&lt;li&gt;# Detector :&amp;nbsp; &amp;nbsp; EIGER X 9M&lt;/li&gt;
	&lt;li&gt;# ZOO mode: mixed scheme (HITO)&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# Multiple small wedge datasets&lt;/li&gt;
	&lt;li&gt;# &amp;#39;CPS1991-05-multi_master.h5&amp;#39; manages 62 datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 5.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;# 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 50 frames / datasets&lt;/li&gt;
	&lt;li&gt;# 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000005.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000006.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000007.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000008.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000009.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000010.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000011.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000012.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000013.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000014.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000015.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000016.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000017.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000018.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000019.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000020.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000021.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000022.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000023.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000024.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000025.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000026.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000027.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000028.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000029.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000030.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_data_000031.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/CPS1991-05-multi_master.h5&lt;/li&gt;
&lt;/ul&gt;

&lt;p&gt;&amp;nbsp;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# &amp;#39;cry-00-??_master.h5&amp;#39; are for &amp;#39;partial helical&amp;#39; datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 40.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 400 frames / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-00_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-01_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-02_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-03_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-04_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-05_master.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-00-06_master.h5&lt;/li&gt;
&lt;/ul&gt;

&lt;p&gt;&amp;nbsp;&lt;/p&gt;

&lt;ul&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# &amp;#39;cry-01-??_master.h5&amp;#39; are for &amp;#39;full rotation helical&amp;#39; datasets&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;# 60.0 deg. / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 0.1 deg. / frame&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 600 frames / datasets&lt;/li&gt;
	&lt;li&gt;#&amp;nbsp; 100 frames in each data file&lt;/li&gt;
	&lt;li&gt;# ** The program could collect &amp;#39;full rotation&amp;#39; helical dataset&lt;/li&gt;
	&lt;li&gt;# but 60 deg. was set for this demonstration.&lt;/li&gt;
	&lt;li&gt;#####################################################&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000001.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000002.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000003.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000004.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000005.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_data_000006.h5&lt;/li&gt;
	&lt;li&gt;hito-CPS1991-05//data/cry-01-00_master.h5&lt;/li&gt;
&lt;/ul&gt;</description>
  </descriptions>
</resource>
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