Enclosed are relevant experimental datasets of: 
“Reaction Environment Design for Multigram Synthesis via Sonogashira Coupling over Heterogeneous Palladium Single-Atom Catalysts” by D. Poier, D. Faust Akl, E. Lucas, A. Rodrigues Machado, G. Giannakakis, S. Mitchell, G. Guillén-Gosálbez, R. Marti, J. Pérez-Ramírez.

This comprises:

- Zenodo_Experimental_Data.xlsx: All datasets concerning the catalytic activity tests, thermogravimetric analysis and gas soprtion experiments.