SAXS data acquired at Diamond Light Source, beamline I22, sm23642

Raw data files are .h5 files which are processed and corrected for transmission using DAWN software (freely available) automatically by Diamond Light Source at the beamline using files 'saxs_Transmission_IvsQ.json' and 'saxs_Transmission_IvsQ_Pipeline.nxs'
Resulting file is a radial integration of the .h5 file which produces a .nxs file with notation i22-FILENUMBER-saxs_Transmission_IvsQ_processed.nxs
Simultaneously .tiff files are produced from the .h5 files using the DAWN software

For ESI Fig 6, the .tiff files are used for analysis and the .nxs files are used to plot the data in ESI 6A and ESI 6B

Data plotting:
ESI Fig 6A.
DAWN was used to export .dat files using the .nxs data
ESI 6A 25degC: i22-543821_saxs_Transmission_IvsQ_processed.nxs
ESI 6A 37degC: i22-543851_saxs_Transmission_IvsQ_processed.nxs
Data was then opened in Excel and normalised by dividing by the maximum value in each dataset

ESI Fig 6B.
DAWN was used to produce subtracted .nxs files using the 'subtract' function. Details are provided in Excel spreadsheet 'ESIFig6A6B_SampleKey'
These files were plotted in DAWN and then exported as .dat files.
Data was then opened in Excel and normalised by dividing by the maximum value in each dataset

Data fitting:
Performed in Axcess using .tiff files. Centre of images is defined as X = 758, y = 84, radial integration performed. Axcess is calibrated using AgbE (File 541469)