GENERAL INFORMATION

Title: How latex film formation and adhesion at the nanoscale correlate to performance of pressure sensitive adhesives with cellulose nanocrystals

Principle Investigator:
Name: Emily D. Cranston
Institution: University of British Columbia
Email: emily.cranston@ubc.ca

Co-investigator:
Name: Elina Niinivaara
Institution: Aalto University and University of British Columbia
Email: elina.niinivaara@ubc.ca

Date of data collection: 2018-08-14 - 2019-03-11
Location of data collection: McMaster University, Hamilton, ON, Canada

DATA AND FILE OVERVIEW

Filename: E0A_from43wt_x10.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with no cellulose nanocrystals. The sample was a 10-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2019-01-21
Filename: E0A_from43wt_x25.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with no cellulose nanocrystals. The sample was a 25-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2019-01-21
Filename: E0A_from43wt_x50.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with no cellulose nanocrystals. The sample was a 50-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2019-01-21
Filename: E0A_from43wt_x75.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with no cellulose nanocrystals. The sample was a 75-fold dilution of the stock suspension which had a solids content of 43 wt%
File created:2019-01-21
Filename: E0A_from43wt_x100.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with no cellulose nanocrystals. The sample was a 100-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2019-01-21

Filename: E0A_Stock_20um.ibw
Description: Atomic force microscopy data (20 x 20 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with no cellulose nanocrystals)
File created: 2018-11-13
Filename: E0A_Stock_75um.ibw
Description: Atomic force microscopy data (75 x 75 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with no cellulose nanocrystals)
File created: 2019-03-11

Filename: E0A_spot10000.ibw
Description: Atomic force microscopy force measurement raw data from first location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with no cellulose nanocrystals)
File created: 2019-01-23
Filename: E0A_spot20000.ibw
Description: Atomic force microscopy force measurement raw data from second location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with no cellulose nanocrystals)
File created: 2019-01-23
Filename: E0A_spot30000.ibw
Description: Atomic force microscopy force measurement raw data from third location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with no cellulose nanocrystals)
File created: 2019-01-23

Filename: E05A_from43wt_x10.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 0.5 wt% cellulose nanocrystals. The sample was a 10-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-12-10
Filename: E05A_from43wt_x25.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 0.5 wt% cellulose nanocrystals. The sample was a 25-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-12-10
Filename: E05A_from43wt_x50.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 0.5 wt% cellulose nanocrystals. The sample was a 50-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-12-07
Filename: E05A_from43wt_x75.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 0.5 wt% cellulose nanocrystals. The sample was a 75-fold dilution of the stock suspension which had a solids content of 43 wt%
File created:2018-12-07
Filename: E05A_from43wt_x100.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 0.5 wt% cellulose nanocrystals. The sample was a 100-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-10-30

Filename: E05A_Stock_20um.ibw
Description: Atomic force microscopy data (20 x 20 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 0.5 wt% cellulose nanocrystals)
File created: 2018-11-13
Filename: E05A_Stock_75um.ibw
Description: Atomic force microscopy data (75 x 75 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 0.5 wt% cellulose nanocrystals)
File created: 2019-03-11

Filename: E05A_spot10000.ibw
Description: Atomic force microscopy force measurement raw data from first location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 0.5 wt% cellulose nanocrystals)
File created: 2019-01-23
Filename: E05A_spot20000.ibw
Description: Atomic force microscopy force measurement raw data from second location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 0.5 wt% cellulose nanocrystals)
File created: 2019-01-23
Filename: E05A_spot30000.ibw
Description: Atomic force microscopy force measurement raw data from third location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 0.5 wt% cellulose nanocrystals)
File created: 2019-01-23

Filename: E1A_from43wt_x10.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 1 wt% cellulose nanocrystals. The sample was a 10-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-12-11
Filename: E1A_from43wt_x25.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 1 wt% cellulose nanocrystals. The sample was a 25-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-12-17
Filename: E1A_from43wt_x50.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 1 wt% cellulose nanocrystals. The sample was a 50-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-11-30
Filename: E1A_from43wt_x75.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 1 wt% cellulose nanocrystals. The sample was a 75-fold dilution of the stock suspension which had a solids content of 43 wt%
File created:2018-11-30
Filename: E1A_from43wt_x100.ibw
Description: Atomic force microscopy data of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film with 1 wt% cellulose nanocrystals. The sample was a 100-fold dilution of the stock suspension which had a solids content of 43 wt%
File created: 2018-08-14

Filename: E1A_Stock_20um.ibw
Description: Atomic force microscopy data (20 x 20 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 1 wt% cellulose nanocrystals)
File created: 2018-11-13
Filename: E1A_Stock_75um.ibw
Description: Atomic force microscopy data (75 x 75 um2 image) of a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 1 wt% cellulose nanocrystals)
File created: 2019-03-11

Filename: E1A_spot10000.ibw
Description: Atomic force microscopy force measurement raw data from first location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 1 wt% cellulose nanocrystals)
File created: 2019-01-23
Filename: E1A_spot20000.ibw
Description: Atomic force microscopy force measurement raw data from second location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 1 wt% cellulose nanocrystals)
File created: 2019-01-23
Filename: E1A_spot30000.ibw
Description: Atomic force microscopy force measurement raw data from third location on a spin coated 2-ethyl hexyl acrylate/n-butyl acrylate/methyl methacrylate latex film of the stock suspension which had a solids content of 43 wt% (with 1 wt% cellulose nanocrystals)
File created: 2019-01-23

Methodological Information

Instrumentation used: MFP-3D Atomic Force Microscope (Asylum Research – Oxford Instruments, Santa Barbara, CA, USA) 
Analysis software: Igor Pro 6.0 running Asylum Research Atomic Force Micrscope software (version 13.17)
Data processing: Images were processed with a standard third-order polynomial flattening. Force measurement rawy data was processed using Igor Pro 6.0 running Asylum Research Atomic Force Micrscope software (version 13.17)
