1H 0.1deg
13C,d6-DMM
---
B0: 96.1 uT
LG:
600 Hz eff.field, angle = ma, ad90 flip
B1adj = -7%
----
4 uT decoupling
SLIC: 0 to 25 Hz in 2 s
ad90: -200 Hz to 0 in 1 s
--
320 mM 13C,d6-DMAD + 5 mM Rh dppb cat
---
12 s pH2 + 18 s N2
--
47%
284 mM